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  • Articles: DFG German National Licenses  (37)
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  • Articles: DFG German National Licenses  (37)
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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 73 (1993), S. 865-870 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The magnetic properties of an Fe73.5Cu1Nb3Si13.5B9 alloy with nanoscale crystalline structure have been investigated as a function of the melt temperature. In the temperature range of 1240 to 1380 °C investigated in the present study, the permeability increases with the melt temperature. This result may be explained in terms of the reduction in the magnetic anisotropy as a function of the melt temperature. This is supported by the results for the remanence ratio, which also increases with melt temperature in a similar manner to the permeability. In the latter part of the work described in this paper, the relationships between the permeability and the coercivity, and the permeability and the remanence ratio have been investigated for the nanocrystalline alloy. It was found that the permeability is correlated more closely to the remanence ratio than the coercivity.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 73 (1993), S. 6591-6593 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The effects of Al on the soft magnetic properties of nanocrystalline Fe73.5−xAlxCu1Nb3Si13.5B9 alloy ribbons are investigated in the composition range of 0≤x≤1.0. The relative initial permeability at 1 kHz is found to increase by the addition of Al, and reaches the peak value at x=0.1. The coercivity decreases, rather significantly, with the Al content in the whole composition range investigated in the present work, the values of the coercivity being 12.5 mOe at x=0 and 9.3 mOe at x=1.0. The magnetic induction at an applied field of 10 Oe, however, decreases moderately by the introduction of Al, possibly due to the dilution effect. The improvement in the soft magnetic properties is considered to result from the reduction in the grain size of the α Fe-Si solid solution phase of the Al-added alloy ribbons, which has been observed by transmission electron microscopy. Another factor may be due to the decrease in the intrinsic magnetocrystalline anisotropy K1 as Al is added to the alloy.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 69 (1991), S. 5921-5923 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The metalloid effect on magnetic properties and microstructures of iron-based alloys with ultrafine grain structures was investigated. For Fe73.5Cu1Nb3(SixB1−x)22.5 (0.5≤x≤0.8) alloys with 10–15-nm grain diameters, the permeability increased with Si content. The alloys with x=0.5 and 0.6 subjected to the optimum heat treatment had two different ferromagnetic phases which were composed of an α-Fe(Si) solid solution with high Curie temperature and an interfacial phase with low Curie temperature. However, in high Si alloys with x=0.7 and 0.8, only a phase with high Curie temperature appeared. This result suggests that in the high Si composition range, a complete transformation from the amorphous phase to the α-Fe(Si) single phase was achieved. The disappearance of the interfacial phase which would certainly disturb the exchange coupling between the α-Fe(Si) phase grains would be considered to be one of the factors for the increased permeability.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 70 (1991), S. 6591-6593 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The effect of ball milling on the magnetic properties of the Pr15Fe80B5 alloy, whose as-cast structure was composed of matrix phase Pr2Fe14B and Pr-rich and α-Fe phases, has been investigated by measuring iHc, thermomagnetic curves, and x-ray diffraction (XRD) patterns. By ball milling using a planetary ball mill up to 96 h, iHc decreased with the amorphization of the matrix and Pr-rich phases. However, subsequent heat treatments gave rise to the marked increase of iHc. The alloy, after 48 h of ball milling and subsequent 600 °C annealing possessed iHc of 17.4 kOe, Br of 5.8 kG, and (BH)max of 6.5 MGOe. This alloy showed sharp diffraction peaks of Pr2Fe14B phase, while the α-Fe phase peak, which persisted through the ball milling process, almost disappeared. The high iHc of the Pr-Fe-B alloy, subjected to optimum milling and subsequent annealing, was attributed to a very fine Pr2Fe14B phase precipitation from the amorphous state and to the effective solution of the α-Fe phase into the matrix phase. Also, a small addition of Cu to the Pr15Fe80B5 alloy was found to increase the coercivity. Further, the alloy milled for 12 h and annealed at 600 °C for 1 h showed iHc of 19.7 kOe, Br of 7.0 kG, and (BH)max of 10.2 MGOe.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 73 (1993), S. 6594-6596 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The magnetic relaxation phenomenon was investigated by using the pulse method for an Fe88Zr7B4Cu1 alloy with nanoscale grain structure, which was prepared by melt quenching and a subsequent annealing. In order to know the relationship between the microstructure and the magnitude of magnetic aftereffect in the nanocrystalline state, annealing temperature dependence of volume fractions of crystalline bcc-Fe and residual amorphous phase was also measured. It was found that disaccommodation occurred in this nanocrystalline alloy, and the intensity of disaccommodation decreased as the fraction of the crystalline bcc-Fe phase increased. Moreover, the jumping field, defined by the magnetic field, at which initial magnetization curve rises abruptly decreased as the fraction of residual amorphous phase was reduced. From the observed results, the magnetic aftereffect was considered to result from the residual amorphous phase.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 64 (1993), S. 2385-2386 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Recently, a new contactless Jc measurement technique by monitoring nonlinear responses from a coil mounted in the proximity of a superconducting film was reported by Classen et al. [Rev. Sci. Instrum. 62, 996 (1991)]. An improved method to measure the nonlinear inductive response is developed using an inductance bridge circuit, which discriminates the third-harmonic signal due to the nonlinearity from those of other origins. Moreover, in this technique, the phase of the third-harmonic signal can be used to determine the critical current.
    Type of Medium: Electronic Resource
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  • 7
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Effects of cooling rate after annealing on the soft magnetic properties were investigated for an Fe88Zr7B4Cu1 alloy with nanoscale grain structure, which was prepared by melt quenching. As the cooling rate increased, the effective permeability improved and the remanence ratio, which indicates the orientation of magnetic anisotropy (degree of pair ordering), decreased. The increase of permeability and decrease of remanence ratio were considered to result from the suppression of the induced magnetic anisotropy. Furthermore, the variation of disaccommodation behaviors with cooling rate was investigated in the Fe88Zr7B4Cu1 nanocrystalline alloy. It was found that the value of D (intensity of disaccommodation) was a little higher for the samples obtained from the high cooling rate than that for the low cooling rate. This result can be explained by domain structure stabilization due to local induced magnetic anisotropy.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 5459-5461 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The amorphous state of ferromagnetic Fe83B9Nb7Cu1 and its nanocrystallization have been studied by x-ray, Mössbauer spectroscopy, and magnetic moment measurements. In the amorphous state at 13 K, the Mössbauer spectrum exhibits an essentially symmetric hyperfine field distribution with a half-width of 72 kOe. The average hyperfine field Hhf(T) of the amorphous state shows a temperature dependence of [Hhf(T)−Hhf(O)]/Hhf(O)=−0.48(T/TC)3/2 u −0.22(T/TC)5/2 for T/TC〈0.7, indicative of spin-wave excitation. The quadrupole splitting just above the Curie temperature TC is 0.43 mm/s, whereas the average quadrupole shift below TC is zero. The Curie and crystallization temperatures are determined to be TC=393 K and Tx=775 K, respectively, for a heating rate of 5 K/min. The occupied area of the nanocrystalline phase at the optimum annealing temperature is about 33%–71%. It is notable that the magnetization of the amorphous phase decreases more rapidly with reduced temperature than those of nanocrystalline ferromagnets, suggesting the presence of the distribution of exchange interactions in the amorphous phase or high metalloid contents. © 1996 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 78 (1995), S. 6151-6156 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Perovskite La1−xCaxMnO3−δ thin films were deposited on MgO(001) substrates using pulsed laser deposition. Effects of deposition conditions, such as laser fluence, substrate temperature, and oxygen pressure, on growth behaviors of the films were investigated over a wide range. Epitaxial La0.7Ca0.3MnO3−δ /MgO thin films were able to be grown in situ under conditions such as 1.5–2.1 J/cm2 laser fluence, 650–750 °C substrate temperature, and 100–300 mTorr oxygen pressure. The oxygen pressure during the deposition is found to be closely related to crystalline orientations of the films. Rutherford backscattering spectroscopy measurements show that the epitaxial La1−xCaxMnO3−δ thin films have compositions similar to those of targets, demonstrating that pulsed laser deposition is a useful technique to get thin films with complicated chemical compositions. The magnetoresistance, −ΔR(6T)/R(0), of the La0.7Ca0.3MnO3−δ /MgO thin film was about −80%, which is smaller than the reported values (i.e., ∼−99.92%) of the La–Ca–Mn–O thin films on LaAlO3 substrates [S. Jin, T. H. Tiefel, M. McCormack, R. A. Fastnacht, R. Ramesh, and L. H. Chen, Science 264, 413 (1994)]. © 1995 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 76 (1994), S. 7021-7023 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The magnetostriction of melt-spun ribbons of Dyx(Fe1−yBy)1−x (x=0.2, 0.25, 0.3; 0≤y≤0.2) alloys is systematically investigated as a function of the wheel speed during melt quenching. As the wheel speed increases from 10 to 50 m/s, the magnetic softness improves with the wheel speed rather continuously for the alloys with the Dy content x=0.2 and 0.25 but it exhibits a maximum at the wheel speed of 30 or 40 m/s for the alloys with the highest B content (x=0.3). The softness also improves with the B content for a fixed wheel speed. Homogeneous and ultrafine grain structure is observed for the first time even in the as-spun state when the ribbons of the alloy Dy0.3(Fe0.8B0.2)0.7 are fabricated at the wheel speed of 30 m/s. The ribbon having the ultrafine grain structure exhibits good magnetic softness together with a high strain.
    Type of Medium: Electronic Resource
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