ISSN:
0935-6304
Keywords:
Gas Chromatography Mass Spectrometry
;
Capillary, glass/Varian, MAT 311A
;
Separation and detection (El, Cl) of some roast coffee constituents
;
Three new phenolic compounds found
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
A roast coffee infusion (nicaragua arabica) was acidified (pH 1,5) with hydrochloric acid and extracted with diethyl ether in a perforator. After evaporation of the solvent the residue was treated with N-methyl-N-trimethylsilyl trifluoroacetamide and analyzed by glass capillary GC/MS. The main components were identified by their electron impact and isobutane chemical ionization mass spectra. 1,2,4-trihydroxy benzene, 1-ethyl-3, 4-dihydroxy benzene and 2,3-dihydroxy toluene were identified as new constituents of roast coffee with possible emetic properties.
Additional Material:
2 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/jhrc.1240010114
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