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Crystal structure of a macrocyclic tetraamine isocyanato zinc(II) complex (1998)

Choi, Ki-Young ; Chun, Kang Moon ; Suh, Il-Hwan

Springer

Journal of chemical crystallography 28 (1998), S. 831-834

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ISSN: 1572-8854

Keywords: Crystal structure ; macrocyclic tetraamine ; isocyanato zinc(II) complex

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The complex, [Zn(L)(NCO)]Cl · 3H2O (1) (L = 3,14-dimethyl-2,6,13,17-tetraazatricyclo[14,4,01.18,07.12]docosane), has been synthesized and structurally characterized. 1 crystallizes in the monoclinic system, space group P21/n with a = 10.530(3), b = 9.315(2), c = 27.188(3) Å, β = 92.58(1)°, V = 2664.1(9)Å3, and Z = 4. The zinc atom is in a distorted squarepyramidal environment with the four nitrogen atoms of the macrocycle and one nitrogen atom of the isocyanate ligand.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1023/A:1021831921283

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