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The crystal and molecular structure of N-(methylsulfonyl)-N-(2,6)-(dimethylphenyl)methanesulfonamide (1994)

Mazhar-Ul-Haque ; Ali, Sk. Asrof

Springer

Journal of chemical crystallography 24 (1994), S. 759-762

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ISSN: 1572-8854

Keywords: Sulfonamide ; methanesulfonanilide ; crystal structure ; molecular structure

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The title compound, crystallizes in the triclinic space group $$P\bar 1$$ witha=8.232(4),b=9.159(2),c=10.230(3)Å. α=74.07(3)°, β=72.50(4)°, γ=63.65(3)° andZ=2. The structure was solved by direct methods and refined by full matrix least squares methods toR=0.054 for 1817 observed reflections. The plane containing the nitrogen and sulfur atoms is perpendicular to the aromatic plane. One of the S−O bonds in each methanesulfonyl group is in nearly eclipsed conformation with the N−C bond.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01666966

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