Digitale Medien
Chester
:
International Union of Crystallography (IUCr)
Journal of synchrotron radiation
5 (1998), S. 905-907
ISSN:
1600-5775
Quelle:
Crystallography Journals Online : IUCR Backfile Archive 1948-2001
Thema:
Geologie und Paläontologie
,
Physik
Notizen:
A compact versatile six-axis goniometer has been built which can be used with the scattering plane vertical or horizontal for anomalous X-ray diffraction and diffraction X-ray absorption fine structure using a tunable X-ray undulator at SPring-8. The diffractometer consists of a four-circle goniometer for the standard ω, 2θ, φ and χ motions and a two-circle goniometer on the 2θ arm for mounting the detector and analyser crystal. The goniometer is controlled via Ethernet, and standard data-acquisition software with a graphical user interface has been developed. A closed-cycle helium cryostat is mounted on the ω axis for temperature-dependent experiments from 330 K to 14 K. Preliminary experiments on a Bi2Sr2CaCu2O8 single crystal demonstrate the performance. Superstructure peaks due to the one-dimensional spatial modulations in the b axis were recorded as a function of temperature above 20 K using an image plate.
Materialart:
Digitale Medien
URL:
http://dx.doi.org/10.1107/S0909049597018098
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