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  • 1
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 42 (1996), S. 87-95 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Liquid-solid fluidization characteristics of irregularly shaped Biobone particles were studied in a fluidized bioreactor column 2.35 m high and 0.1 m dia. The wet biobone particles had a density of 1,890 kg/m3. Two size ranges were studied: 1.70-2.36 mm and 1.25-2.36 mm. The Biobone is a natural cheap material composed of collagen, which is a strong protein structure, embedded with microcrystals of hydroxyapatite and calcium phosphate, and it is an excellent matrix of commercial importance used for the immobilization of enzymes, whole cells and other biocatalysts. Fluidization characteristics of Biobone particles, which include measurements of pressure drops, holdups, minimum fluidization velocities, particle entrainment, and residence time distributions at different water superficial velocities, are reported. Because of the highly irregular shape of Biobone particles, new fluidization behavior was observed, which was much different from the fluidization behavior of spherical particles reported in the literature. A new channeling index, Ic, is proposed to quantify the channeling characteristics of fluidized Biobone particles, and a new parameter, α, was developed to distinguish the transition between fixed and fluidized states of the Biobone particles.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 32 (1986), S. 233-238 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: A model describing the entrainment of solid particles from gas-fluidized beds of mixed-size particles is proposed. It was tested with the limited experimental data published to date and was shown to be superior to existing models and correlations. The model demonstrates that the concentration of very fine particles in the bed can have a significant effect on entrainment.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 38 (1992), S. 1206-1212 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Inclining a fluidized bed column by as little as 1.5 degrees greatly affects the bed characteristics. The bed contracts, the particle-liquid mass-transfer and heat-transfer coefficients increase by up to 30%, and the gas-liquid mass-transfer coefficient can either be increased by up to 15% or decreased by up to 20%.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    Biotechnology and Bioengineering 46 (1995), S. 388-392 
    ISSN: 0006-3592
    Keywords: volumetric mass transfer coefficient ; oxygen uptake rate ; probe response time ; dynamic gas out-gas in method ; Chemistry ; Biochemistry and Biotechnology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: There are many dynamic methods for measuring the volumetric mass transfer coefficient. The “gas out-gas in” method can directly determine the volumetric mass transfer coefficient in a bioreactor system and provide estimates of the volumetric microbial oxygen uptake rate and the average oxygen saturation concentration at the gas-liquid interface. The errors on these parameters are large if the dissolved oxygen probe response time is not considered. For reliable measurements, deconvolution of the oxygen probe measurements must be made. © 1995 John Wiley & Sons, Inc.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 43 (1997), S. 1180-1189 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Accurate detection of minimum liquid fluidization is essential to the successful operation of gas-liquid-solid fluidized beds, especially when particle or liquid properties evolve. A gas-liqid-solid system of 3-mm glass beads exhibits three distinct flow regimes as the liquid velocity is increased: compacted, agitated and fluidized-bed regmes. Measurements showed that the bed is not fluidized in the agitated bed regime. Pressure gradient and bed height measurements do not provide the minimum liquid fluidization velocity; instead, they offer the velocity between the compacted and agitated bed regimes. Time-averaged signals are not reliable for determining the minimum liquid fluidization velocity. It can be obtained from the standard deviation, the average frequency, the Hurst exponent and the V statistic of the cross-sectional average conductivity, which can be measured under many industrial conditions.
    Additional Material: 16 Ill.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 43 (1997), S. 1469-1479 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Fast circulating fluidized-bed reactors are used for many applications, both in riser and downer modes. Typical resisdence times are in the order of a few hundreds of milliseconds. A good understanding of initial gas-solids contact must be reached to realize the full potential of such reactors. Effective and stable gas-solids mixing chambers were identified from the singals of simple and robust probes, which could be used in industrial and pilot plants. Criteria based on cross correlation or Hurst analysis provided consistent results. Although this study used simplified momentum probes, the criteria it developed can be applied to the signal of any fast-response sensor which is affected by local hydrodynamics. Temperature, capacitance, ultrasonic, or γ-ray absorption measurements could be used. Gas or liquid-liquid mixing chambers could also be optimized with the same criteria.
    Additional Material: 19 Ill.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 43 (1997), S. 1904-1908 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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