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  • 1
    Digitale Medien
    Digitale Medien
    Determination of Particle Size and Shape during the Hydrolysis of Pb(Zr0.3Ti0.7)O3 Precursor Solutions (1998)
    Springer
    Journal of sol gel science and technology 11 (1998), S. 141-152 
    Details
    ISSN: 1573-4846
    Schlagwort(e): precursor chemistry ; lead zirconate titanate ; hydrolysis ; PCS ; SAXS
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Abstract The formation and growth of polymeric particles during the hydrolysis and condensation of PbZr0.3Ti0.7 O3 (PZT 30/70) sol-gel precursor solutions have been investigated by using photon correlation spectroscopy (PCS), small angle X-ray scattering (SAXS) and by measuring their rheological properties. The measurements showed that the growth of the particles in the transition of PZT sol to gel followed a simple polymerisation process. Solution A (containing ‘by-products’) and Solution B (‘by-products’ removed) displayed a similar plot of logarithmic viscosity against logarithmic time, indicating that the particles in both solutions have similar structures after hydrolysis. The changes in viscosity and particle size with time were described by single logarithmic growth models. However, the increasing rate of logarithmic particle size in Solution B is higher than that in Solution A. A model for the form of the aggregates is discussed which is applicable to PZT organometal-particle aggregation process in systems with acetic acid as a modifier.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1023/A:1008641429895
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  • 2
    Digitale Medien
    Digitale Medien
    A Comparison of the Nanostructure of Lead Zirconate, Lead Titanate and Lead Zirconate Titanate Sols (1999)
    Springer
    Journal of sol gel science and technology 15 (1999), S. 13-22 
    Details
    ISSN: 1573-4846
    Schlagwort(e): precursor chemistry ; lead zirconate titanate ; hydrolysis ; PCS ; SAXS
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Abstract Sol-gel processing has been widely used for the fabrication of lead zirconate titanate (PZT) thin films. To successfully and consistently make high quality thin films for different applications, we must develop a fundamental understanding of the structures of the sols. In this study, the characters of lead titanate (PT) and lead zirconate (PZ)sols were studied by measuring the rheological properties and particle sizes in them and comparing their behaviours. The average particle sizes in unhydrolysed PT, PZ and PZT sols are 11.5, 1.0, and 6.0 nm, respectively. PT sol has the highest rate of hydrolysis. It gels at about 24 h after hydrolysis. PZ and PZT sols have a quite similar feature in hydrolysis. The reasons for the differences in the hydrolysis behaviour of the different types of sol are discussed in terms of a model which indicates that the inhomogeneous sols consist of 5 to 6 nm PT particles surrounded by much smaller PZ particles, which tend to dominate the sol behaviour.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1023/A:1008759520087
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  • 3
    Digitale Medien
    Digitale Medien
    A diallel analysis of heterosis in elite hybrid rice based on RFLPs and microsatellites (1994)
    Springer
    Theoretical and applied genetics 89 (1994), S. 185-192 
    Details
    ISSN: 1432-2242
    Schlagwort(e): Oryza sativa ; Hybrid vigor ; Molecular marker ; Yield
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Abstract Hybrid rice has contributed significantly to the dramatic increase of rice production in the world. Despite this, little attention has been given to studying the genetic basis of heterosis in rice. In this paper, we report a diallel analysis of heterosis using two classes of molecular markers: restriction fragment length polymorphisms, (RFLPs) and microsatellites. Eight lines, which represent a significant portion of hybrid rice germ plasm, were crossed in all possible pairs, and the F1s were evaluated for yield and yield component traits in a replicated field trial. The parental lines were surveyed for polymorphisms with 117 RFLP probes and ten microsatellites, resulting in a total of 76 polymorphic markers well-spaced in the rice RFLP map. The results indicated that high level heterosis is common among these crosses: more than 100% midparent and 40% better-parent heterosis were observed in many F1s, including some crosses between maintainer lines. Heterosis was found to be much higher for yield than for yield component traits, which fits a multiplicative model almost perfectly. Between 16 and 30 marker loci (positive markers) detected highly significant effects on yield or its component traits. Heterozygosity was significantly correlated with several attributes of performance and heterosis. Correlations based on positive markers (specific heterozygosity) were large for midparent heterosis of yield and seeds/panicle and also for F1 kernel weight. These large correlations may have practical utility for predicting heterosis.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/BF00225139
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  • 4
    Digitale Medien
    Digitale Medien
    Molecularmarker diversity and hybrid sterility in indica-japonica rice crosses (1997)
    Springer
    Theoretical and applied genetics 95 (1997), S. 112-118 
    Details
    ISSN: 1432-2242
    Schlagwort(e): Key words Diallel cross ; Hybrid rice ; Oryza sativa ; Restriction fragment length polymorphism (RFLP) ; Simple sequence repeat (SSR)
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Abstract  The partial sterility of hybrids between the indica and japonica rice subspecies of Asian cultivated rice is a serious constraint for utilizing inter-subspecific heterosis in hybrid rice breeding. In this study, we have investigated the relationship between molecular-marker polymorphism and indica-japonica hybrid fertility using a diallel set involving 20 rice accessions including 9 indica and 11 japonica varieties. Spikelet fertility of the resulting 190 F1s and their parents was examined in a replicated field trial. Intra-subspecific hybrids showed much higher spikelet fertility than inter-subspecific hybrids except in crosses involving wide-compatibility varieties. The parents were surveyed for DNA polymorphism using 96 RFLP and ten SSR markers, which revealed extensive genetic differentiation between indica and japonica varieties. A large number of markers detected highly significant effects on hybrid fertility. The chromosomal locations for many of the positive markers coincided well with previously identified loci for hybrid sterility. The correlation between hybrid fertility and parental distance was low in both intra- and inter-subspecific crosses. The results suggest that the genetic basis of indica-japonica hybrid sterility is complex. It is the qualitative, rather than the quantitative, difference between the parents that determines the fertility of hybrids.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/s001220050538
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