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Enzymatic resolution of alkyn-3-ols in non-aqueous medium (1996)

Sharma, A. ; Sankaranarayanan, S. ; Chattopadhyay, S.

Springer

Biotechnology letters 18 (1996), S. 1391-1394

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ISSN: 1573-6776

Source: Springer Online Journal Archives 1860-2000

Topics: Process Engineering, Biotechnology, Nutrition Technology

Notes: Summary Resolution of alkyn-3-ols has been achieved using a lipase from Candida rugosa to esterify the alcohols with trifluoroethyl butyrate in hexane to give the (S)-alcohols and the (R)-esters. Subsequent reacylation of the product alcohols and alcoholysis of the esters with 1-butanol furnished the (S)-alcohols with good (86–91% ees) and the (R)-butyrate with moderate enantiomeric purities (62–64% ees).

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00129341

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