ISSN:
1572-9001
Keywords:
X-ray diffraction
;
monoclinic twinning
;
crystal structure determination
;
dioxaborolane
;
tetramethylurea adduct
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Abstract The title compound crystallizes in the monoclinic space groupP21/c. Twinning occurs between domains sharing thehk0 zone. The indices of imprecise intensity data were interpreted successfully. A subset of these data could be corrected and used in structure determination together with single-crystal intensity data of the predominant domain, whereas the remaining superposition data were excluded from refinement. Structure solution converged at satisfactory values ofR=0.082,R w=0.074. The structure consists of isolated Lewis acid base adducts.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF02278695
