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  • Artikel: DFG Deutsche Nationallizenzen  (5.452)
  • 1970-1974  (5.452)
  • Physics  (2.547)
  • Analytical Chemistry and Spectroscopy  (2.128)
  • Engineering  (489)
  • Engineering General  (489)
  • Rat  (288)
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  • Artikel: DFG Deutsche Nationallizenzen  (5.452)
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  • 101
    Digitale Medien
    Digitale Medien
    Discrete (Legendre) orthogonal polynomials - a survey (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 743-770 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The discrete (Legendre) orthogonal polynomials, (DLOP's) are useful for approximation purposes. This set of mth degree polynomials {Pm(K, N)} are orthogonal with unity weight over a uniform discrete interval and are completely determined by the normalization Pm(O, N) = 1. The authors are employing these polynomials as assumed modes in engineering applications of weighted residual methods. Since extensive material on these discrete orthogonal polynomials, and their properties, is not readily available, this paper is designed to unify and summarize the presently available information on the DLOP's and related polynomials. In so doing, many new properties have been derived. These properties, along with sketches of their derivation, are included. Also presented are a representation of the DLOP's as a product of vectors and matrices, and an efficient computational scheme for generating these polynomials.
    Zusätzliches Material: 5 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080406
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  • 102
    Digitale Medien
    Digitale Medien
    Variational principles and the patch test (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 783-801 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The patch test is shown to be contained in the variational formulations of the finite element methods at the assembling level, all of which require the vanishing of the virtual work of interface connection loads. By a systematic introduction of stress generating functions, attention is drawn to the fact that any given finite element model can be assembled in two different ways: either by identification of a set of boundary displacements (leading to the direct stiffness method), or by identification of a set of local stress function values (leading to the dual direct flexibility method). Looking at any conjugate couple (generalized displacement-generalized surface traction) at an interface, one is strongly transmitted, the other weakly. Discretization of the zero virtual work condition at an interface of plate bending models, by means of Legendre polynomial expansions, allows a systematic construction of so-called ‘non-conforming’ elements that pass the patch test. They are in fact identified with weakly conforming, but strongly diffusive, hybrids, and the lowest degree element (quadratic) is in fact the Morley constant-moment element. Examples are given for higher degree displacement fields.The case of plate stretching elements can be handled by duality, the difficulties being here associated with the requirements for diffusivity. Non-diffusive elements that pass the zero interface virtual work test can be constructed systematically and are identifiable with weakly diffusive, but strongly conforming, hybrids of the type first proposed by T. H. H. Pian.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080408
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  • 103
    Digitale Medien
    Digitale Medien
    Masthead (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974) 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080101
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  • 104
    Digitale Medien
    Digitale Medien
    Body oriented (natural) co-ordinates for generating three-dimensional meshes (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 27-43 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: Body oriented co-ordinates are defined for three-dimensional regions bounded by six surfaces. From this definition of body oriented co-ordinates, two transformations are derived: 1Body oriented surface co-ordinates to the Cartesian co-ordinates, and2Body oriented co-ordinates for a three-dimensional region to Cartesian co-ordinates.With these transformations a mesh generator is developed based on the principle that the mesh required to describe a region will be calculated according to the placement of the discrete points that describe the boundary edges. This is accomplished with two versions of the mesh generator: the surface generator and the volume generator. The surface generator maps the four boundaries of the surface onto the four boundaries of a unit square. Next, the interior points for the surface mesh are established in the mapped space. Then, using the first transformation, the co-ordinates for the surface nodal points are calculated. Similarly, the volume generator maps the six surfaces of the body onto the surfaces of a unit cube, establishes the interior nodal points in the mapped space, and using the second transformation, calculates the co-ordinates for the interior nodal points.
    Zusätzliches Material: 11 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080104
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  • 105
    Digitale Medien
    Digitale Medien
    Finite elements in the solution of electromagnetic induction problems (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 359-367 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: This paper describes a method of solving electromagnetic induction problems by means of the finite element technique. A variational equation associated with the differential equation for the vector potential is formulated and solved via the concept of finite elements. Sinusoidal driving currents and linear, isotropic, but inhomogeneous media are assumed. A typical example is included in order to illustrate the suggested solution technique.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080213
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  • 106
    Digitale Medien
    Digitale Medien
    Mesh generation program for highway excavation cuts (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 369-394 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The mesh generation program described here generates the nodes and the elements for excavated highway slopes, applies boundary conditions, searches for the nodes and the elements in each layer excavated and plots the mesh with the numbering of nodes, elements and material types.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080214
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  • 107
    Digitale Medien
    Digitale Medien
    Finite element analysis of elasto-plastic shellsThis research was sponsored by AB Volvo, Göteborg, Sweden. (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 415-424 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A finite element analysis applicable to elasto-plastic shells of arbitrary shape is presented. Small-deflection behaviour of thin shells subjected to monotonically increasing static loads is considered. The material is assumed to be originally isotropic, following the von Mises yield criterion and the Prandtl-Reuss flow rule. A flat triangular element with twelve degrees of freedom is used in the analysis. Within each element both membrane forces and bending moments are assumed to be constant. Some numerical results are included to illustrate the merits of the element.
    Zusätzliches Material: 8 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080217
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  • 108
    Digitale Medien
    Digitale Medien
    On the treatment of boundary conditions by the method of artificial parametersThe research reported on here was supported by the Office of Naval Research (Contract NR 064-452). (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 425-429 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A procedure to deal with various boundary conditions in the Rayleigh-Ritz method is discussed herein, namely, the method of artificial parameters. The method is then applied to solve a simple string problem; results obtained compare very nicely with exact solutions.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080218
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  • 109
    Digitale Medien
    Digitale Medien
    A discussion on a modified conjugate gradient method (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 431-432 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080221
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  • 110
    Digitale Medien
    Digitale Medien
    The rectangular plane stress element by Turner, Pian and Wilson (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 433-437 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: One of the first finite elements presented was that by Turner et al.1 Pian2 presented a hybrid plane stress element and Wilson et al.3 presented a non-conforming displacement element. It is shown that the three resulting stiffness matrices are identical.
    Zusätzliches Material: 2 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080223
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  • 111
    Digitale Medien
    Digitale Medien
    Local and global smoothing of discontinuous finite element functions using a least squares method (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 461-480 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The concepts and potential advantages of local and global least squares smoothing of discontinuous finite element functions are introduced.The relationship between local smoothing and the ‘reduced’ integration' technique is established.Examples are presented to illustrate the application of the two smoothing techniques to the finite element stresses from several structural analysis problems.The paper concludes with some practical recommendations for discontinuous finite element function smoothing.
    Zusätzliches Material: 12 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080303
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  • 112
    Digitale Medien
    Digitale Medien
    Finite element solutions for an equilateral triangle (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 495-501 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: In a two-dimensional space of points on an equilateral triangle grid, a single difference equation holding at each node is found from the finite element formulation of the wave equation for all published polynomial orders of the functional expansion. Assuming homogeneous boundary conditions on any equilateral triangle whose edges and vertices pass through the grid points, the eigensolutions of the difference equation are found exactly and thus provide an excellent test problem for the programmer or engineer. The advantage of the present method over other formulations is that the number of linear operations required to produce the difference equation is minimal.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080305
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  • 113
    Digitale Medien
    Digitale Medien
    Reply to preceding discussion (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 429-430 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080219
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  • 114
    Digitale Medien
    Digitale Medien
    A discussion on the density of finite element matricesJ. Alan George, ‘On the density of finite element matrices’, Int. J. num. Meth. Engng, 5, 297-300 (1972). (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 432-432 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080222
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  • 115
    Digitale Medien
    Digitale Medien
    Mathematics for engineers and scientists, A. C. Bajpai, I. M. Calus and J. A. Fairley, Wiley, London, 1973. (Two volumes), Price: Vol. 1, £3.25, Vol. 2, £3.75 (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 438-438 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080224
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  • 116
    Digitale Medien
    Digitale Medien
    Stresses in nearly incompressible materials by finite elements with application to the calculation of excess pore pressures (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 443-460 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A number of problems are analysed by the displacement method to assess the stress accuracy at very low compressibilities. ‘Parabolic’ isoparametric elements are used. It is found that the mean stress becomes grossly in error at the centre and edges of each element as the compressibility is reduced whereas the deviatoric stress components do not. All stress components retain good accuracy at the ‘reduced’ integration sampling points (2 × 2 Gauss). ‘Exact’ integration yields a similar stress distribution to ‘reduced’ but the mean stress is grossly in error at the integration points (3 × 3 Gauss). Exceptions, however, occur.These findings are interpreted, and a rule for predetermining whether or not accurate stresses can be obtained at the integrating points is suggested. Thus it is shown that the displacement method is suitable for analysing materials which for practical purposes are incompressible.A procedure is then presented for analysing porous media-both linear and non-linear-by separating the stiffness into ‘effective’ and ‘pore fluid’ components. This allows excess pore pressure to be calculated explicitly. Applications to saturated soils are given which make use of the findings of the first part of the paper.
    Zusätzliches Material: 10 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080302
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  • 117
    Digitale Medien
    Digitale Medien
    Spline-blended approximation of Hartmann's flow (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 529-536 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The steady state flow problem known in magnetohydrodynamics as Hartmann's flow is converted into variational formulation and is given an approximate solution by means of the spline blended interpolation technique. The equations of motion consist of two coupled potential flow problems with homogeneous boundary conditions. The spline blended interpolation method is reduced here, because of the shape of the domain, to a cartesian product of cardinal splines with trigonometric or ordinary polynomials. ‘Exact’ boundary conditions are presented by the blending technique. The numerical results indicate that high accuracy is possible with relatively few unknowns.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080309
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  • 118
    Digitale Medien
    Digitale Medien
    Finite element solution of non-linear heat conduction problems with special reference to phase change (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 613-624 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The paper presents a generally applicable approach to transient heat conduction problems with non-linear physical properties and boundary conditions. An unconditionally stable central algorithm is used which does not require iteration.Several examples involving phase change (where latent heat effects are incorporated as heat capacity variations) and non-linear radiation boundary conditions are given which show very good accuracy.Simple triangular elements are used throughout but the formulation is generally valid and not restricted to any single type of element.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080314
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  • 119
    Digitale Medien
    Digitale Medien
    Calculation of transient temperature fields with finite elements in space and time dimensions (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 625-631 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A program is demonstrated which apart from linear finite elements in time also includes elements with shape functions of the second and third degree. The algorithm for discretization in the time dimension is described and, using the example of a parabolic time element, the coefficients required to form the global system are given. By various test examples the efficiency of the process is examined by comparison with the customary difference method. Generally, with finite elements in time, the solution has better stability. Comparing the time required for calculation with the accuracy of the solution it would appear that in examining problems where boundary conditions are constant in time, higher order time elements are no improvement over the linear time element. However, for the purpose of reproducing periodic processes, higher order time elements offer an advantage in that one is not limited to linear variations of the boundary conditions within the element. Thus, for example, the temperature curve for parabolic variation of the surface temperature can be reproduced with close approximation by two time elements per period and a shape function of the third degree.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080315
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  • 120
    Digitale Medien
    Digitale Medien
    Announcement (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 676-676 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080322
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  • 121
    Digitale Medien
    Digitale Medien
    Steady magnetohydrodynamic flow past a circular cylinder (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 771-781 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The steady two-dimensional, viscous, electrically conducting flow around a circular cylinder is investigated. The flow and magnetic field are uniform and parallel at large distances from the cylinder. The equations and boundary conditions are derived for arbitrary values of R, Rmand β, where R is the Reynolds number, Rm the magnetic Reynolds number and β, the ratio of the square of the Alfvén speed to the square of the main stream speed. Because of the large number of parameters involved, the numerical solution is restricted to R = 40, Rm = 1 and infinity and 0 ≤ β ≤ 4. Also the cylinder is taken to be a perfect conductor, this avoids having to compute the magnetic field within the cylinder.The numerical computations for the non-magnetic case, i.e. β = 0, are presented and are found to be in good agreement with existing results. The effect of increasing the strength of the magnetic field (i.e. increasing β) on the drag coefficient, the size and position of the standing vortex and the increasing effect of the upstream propagation of disturbances are examined.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080407
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  • 122
    Digitale Medien
    Digitale Medien
    A second order finite element method for the one-dimensional Stefan problem (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 811-820 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: We describe a finite element method for the one-dimensional Stefan problem. The elements are quadrilaterals of the space-time plane which are determined at each time-step in relation with the position of the free boundary. The method appears as a generalization of the classical Crank-Nicolson scheme, since it is identical to this scheme in the case of rectangular elements; it has the advantage of providing a simple and accurate determination of the free boundary. Numerical experiments show that the order of accuracy is equal to 2.
    Zusätzliches Material: 2 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080410
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  • 123
    Digitale Medien
    Digitale Medien
    Least squares finite element analysis of laminar boundary layer flows (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 865-876 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: Based on the least squares error criterion, a class of finite element is formulated for the numerical analysis of steady state viscous boundary layer flow problems. The method is essentially a discrete element-wise minimization of square and weighted residuals which arise from the attempts in approximately satisfying boundary layer equations. An iterative linearization scheme is developed to circumvent the mathematical difficulties posed by the non-linear boundary layer equations. It results in a process of successive least squares minimizations of residual errors arising from satisfying a set of linear differential equations. A mathematical justification for the method is presented. A major feature of the method lies in the linearization approach which renders non-linear differential equations amenable to linear least squares finite element analysis. Another important feature rests on the proposed finite element formulation which preserves the symmetric nature of finite element matrix equations through the use of the least squares error criterion. Numerical examples of viscous flow along a flat plate are presented to demonstrate the applicability of the method as well as to illuminate discussions on the theoretical aspects of the method.
    Zusätzliches Material: 8 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080413
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  • 124
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    Numerical solution of partial differential equations, Edited by J. Gram, D. Reidel, Amsterdam, 1973, Price : ƒ62 (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 917-917 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080417
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  • 125
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    Imperfections in axially loaded plane frames (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 847-864 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A finite beam-column element computer program for the structural failure analysis of proportionally loaded skeletal plane frames is described. The program, which is based on an iterative stiffness approach, provides for non-linear elastic or plastic-non-linear elastic behaviour. Particular attention is given to the incorporation into the analysis of geometrical imperfections, return of elasticity at plastic hinges and negative frame stiffness. The effect of lack-of-fit displacements on the load-deflection path and failure load of frames that carry relatively large axial loads is described in general terms. The theory is developed further through the application of the computer program to two examples which show the necessity for the allowing for the effect of imperfections when designing axially loaded redundant frames.
    Zusätzliches Material: 9 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080412
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  • 126
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    Eigenproblem solution of damped structural systemsThis paper presents the results of one phase of research carried out at the Jet Propulsion Laboratory, California Institute of Technology, under Contract No. NAS 7-100, sponsored by the National Aeronautics and Space Administration. (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 877-911 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: This article presents an efficient numerical algorithm a complete listing of the associated computer program, developed for the eigenproblem solution of discrete damped structures, including spinning ones. The numerically stable procedure is based on a combined Sturm sequence and inverse iteration technique, which fully exploits the banded form of the relevant matrices and proves to be most substantially economical when compared to similar existing softwares. Numerical results are presented for representative structures, solved by the present computer program written in FORTRAN V for the JPL UNIVAC 1108 computer.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080414
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  • 127
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    A note on some variational statements for the slow flow of a Navier-Poisson fluid (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 17-25 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: Three variational statements for the slow time-independent flow of a Navier-Poisson fluid are derived. All of these statements are suitable as the bases of finite elements. The first statement is applied successfully to several flow situations.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080103
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  • 128
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    On some numerical schemes for the solution of wave propagation problems (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 91-102 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: This paper deals with the numerical solution of wave propagation problems in general although the primary area of interest is elastodynamics. The work is applicable to a variety of wave propagation phenomena of classical physics. Explicit schemes of Strang type are used, which allow many simplifications over existing methods. The Strang schemes allow in a very real but perhaps unexpected way the splitting of the elasticity operator.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080108
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  • 129
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    Finite elements formulated by the weighted discrete least squares method (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 71-90 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: By use of the least squares error criterion, an alternate finite element formulation is presented. The method is based on the discrete or element-wise minimization of square and weighted differential equation residuals which are expressed in terms of element nodal quantities. In order to overcome the stringent inter-element continuity requirement, a major stumbling block, on the element trial functions two practical schemes are proposed. One is the reduction of the original governing differential equation to a system of equivalent first order differential equations; the other is a method of smoothing discontinous trial functions. The latter essentially relaxes the continuity requirement and yields efficient non-conforming finite elements. This paper also demonstrates the use of constant weights which significantly improves the rates of convergence. Several numerical examples illustrate the proposed method. From these examples, it may be concluded that the use of constant weights and the relaxation of the inter-element continuity requirement are two indispensable features of the weighted discrete least square method.
    Zusätzliches Material: 17 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080107
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  • 130
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    A direct matrix method for the elastic stability analysis of deep circular arches (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 119-138 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A direct method is described for the evaluation of the critical loads on deep circular arches having various forms of end support. The method is applicable to arches of non-uniform flexural rigidity and may cater for arbitrary forms of applied load distribution. The results calculated for two examples are given, and compared with those obtained analytically and experimentally by other investigators. A complete listing of a computer program for one of the examples is provided in the Appendices.
    Zusätzliches Material: 10 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080111
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  • 131
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    Torsion of axi-symmetric solids of variable diameter - including acceleration effects (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 195-198 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A finite element method for the analysis of axisymmetric bodies in torsion is presented. The effects of an angular acceleration about the axis of symmetry is included. The accuracy of the method is tested against experimental results available for a stepped shaft and finally the problem of an accelerating shaft-turbine disc system is considered.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080114
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  • 132
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    Flow of plastic and visco-plastic solids with special reference to extrusion and forming processes (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 1-16 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: When large, progressive, deformation occurs under plastic or visco-plastic conditions, elastic deformations are negligible and the material flows in a viscous manner. The flow is non-Newtonian and the viscosity is a function of the current strain rates. An effective numerical treatment of such non-Newtonian flow by the finite element method is indicated here and is illustrated by examples of an extrusion process for which approximate slip line solutions are known.The methodology is extended to the solution of transient, quasi-static situations and coupling with thermodynamic equations is discussed.A stream function formulation of the problem is used.
    Zusätzliches Material: 11 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080102
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  • 133
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    A finite element analysis for time-dependent problems (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 55-69 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The finite element method is applied to dynamic linear viscoelastic analysis. The arising system of differential equations is integrated by means of the Laplace transformation. The direct numerical evaluation of the inversion integral seems to be appropriate in case of vibrational problems. The method is applied to examples of transient vibrations of elastic bodies. Initial conditions and arbitrary damping matrices can be considered.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080106
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  • 134
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    On the accuracy of finite element solutions to the transient heat-conduction equation (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 103-110 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: This paper discusses three numerical integration schemes connected with a finite element solution to the transient heat-conduction equation. The main emphasis is on the achievable accuracy. A simple recurrence relation derived from the Galerkin process is suggested for the treatment of fast-varying boundary conditions as being significantly better than the usual Crank-Nicholson scheme in matters of short-time accuracy.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080109
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  • 135
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    Matrix structural analysis with mixed variables (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 167-194 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: Use of mixed force and displacement variables may be the key to a reliable solution of many physical problems. For the analysis of elastic structures with large rigid motion the displacement method may fail due to illconditioning, but use of mixed variables (diacoptics) may work due to the possibility of using relative displacements within substructures. Analysis with mixed variables complicates the topology (the number of nodes and the number of variables at the nodes may vary in the same problem) so a careful study of the system analysis is required. Some general computer routines are given for handling topology, merging and solution of the sparse system equation. The solution routine handles constraints in a rational way and can also be used for decomposition of the system equation or for releasing inner nodes in superelements.
    Zusätzliches Material: 13 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080113
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  • 136
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    Digitale Medien
    The static condensation algorithm (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 198-203 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The application of the static condensation method is discussed in general. The technique is presented as an extension of the Gauss elimination algorithm. An efficient FORTRAN subroutine is given which simultaneously reduces both the stiffness matrix and the stress-displacement transformation matrix.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080115
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  • 137
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    Announcement (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 212-212 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080119
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  • 138
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    Digitale Medien
    Masthead (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974) 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080201
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  • 139
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    An integrated sequential solver for large matrix equations (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 227-248 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: An integrated sequential computer programme for the solution of large linear algebraic systems encountered in the discrete analysis of complex structures using finite element idealization is described. The programme uses an algorithm based on Gauss elimination for solution and is independent of the possible symmetric nature of the system matrix thus enhancing the applicability of the programme for systems with unsymmetric coefficient matrices. The present programme can handle large band widths and the core memory is used efficiently for all feasible problem sizes. A FORTRAN print-out of the programme with relevant explanatory comments and a full notation list are appended.
    Zusätzliches Material: 2 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080204
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  • 140
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    Cycle bases for the flexibility analysis of structures (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 521-528 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: Two methods are presented for the automatic selection of a cycle basis leading to a sparse flexibility matrix for the analysis of rigid-jointed skeletal structures.The first method having a local approach forms a maximal set of admissible minimal cycles, while the second having a global approach constructs admissible minimal cycles on the ordered chords of a shortest route tree. A cycle ordering algorithm is also given to reduce the band width of the corresponding flexibility matrix.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080308
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  • 141
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    The application of quasilinearization to non-linear systems (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 589-611 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: This paper presents a method of solving systems of simultaneous non-linear partial differential equations using the method of lines and the method of quasilinearization-superposition in combination. The advantages of the method over those methods more generally used are discussed and an example of the application of the method to the two-dimensional momentum and energy equations considering temperature-dependent and/or shear-rate dependent viscosity is given.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080313
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  • 142
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    Digitale Medien
    On the accuracy of certain C0 continuous finite element representations (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 649-657 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080317
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  • 143
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    An application of least squares to one-dimensional transient problems (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 633-647 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The method of ‘least squares’, which falls under the category of weighted residual processes, is applied as a time-stepping algorithm to one-dimensional transient problems including the heat conduction equation, diffusion-convection equation, and a non-linear unsaturated flow equation. Comparison is made with other time-stepping algorithms, and the least squares method is seen to offer definite advantages.
    Zusätzliches Material: 8 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080316
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  • 144
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    Computational methods for matrix eigen problems A. R. Gourlay and G. A. Watson, Wiley, London, 1973. 130 Pages. Price: £3.50 (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 676-676 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080321
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  • 145
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    Automatic triangulation of arbitrary planar domains for the finite element method (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 679-696 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The object of this paper is to describe a new algorithm for the semi-automatic triangulation of arbitrary, multiply connected planar domains. The strategy is based upon a modification of a finite element mesh genration algorithm recently developed. 1 The scheme is designed for maximum flexibility and is capable of generating meshes of triangular elements for the decomposition of virtually any multiply connected planar domain. Moreover, the desired density of elements in various regions of the problem domain is specified by the user, thus allowing him to obtain a mesh decomposition appropriate to the physical loading and/or boundary conditions of the particular problem at hand. Several examples are presented to illustrate the applicability of the algorithm. An extension of the algorithm to the triangulation of shell structures is indicated.
    Zusätzliches Material: 19 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080402
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  • 146
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    A finite element analysis of general deformation of sheet metals (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 731-741 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A polynomial shape function of triangular elements for finite element analysis of general deformation of sheet metals with or without orthotropic anisotropy is proposed. And general formulation for large deformation and large strain analysis with non-linearity of material property, say plasticity, is given. Some numerical examples are examined with respect to hydraulic bulging.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080405
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  • 147
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    A finite element analysis in polar co-ordinates of the Saint Venant torsion problem (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 713-729 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A characteristic feature of the variational functionals for several boundary value problems in polar co-ordinates is the fact that one independent variable occurs explicitly in the denominator. Therefore, the coefficients of the finite element equations for sectors of circular ring shaped elements are not constants but functions of the distance of the elements from the origin of co-ordinates.1 We name them coefficient functions. In order to show the particular aspects of the calculations in terms of polar co-ordinates we deal here with the solution of the torsion problem by bilinear and bicubic Hermitian interpolation.The finite element equations are arranged according to Schaefer2 in the form of block which can easily be transformed into ‘stars’3 or molecules4,5 similar to those used in finite difference methods. The origin of co-ordinates requires a special consideration, firstly because of the coincidence of several nodes at that point and secondly because of the divergent behaviour of some coefficient functions. It turns out to be advantageous for the numerical calculations to expand the coefficient functions in power series. Besides, the expansions are required to deduce the equations for rectangular elements by limiting processes. The twisting moments and shearing stresses calculated for several cross sections illustrate the numerical suitability of the method. The finite element values are compared partly with exact solutions and partly with experimental results obtained by a moiré method using Prandtl's soap film analogy.6 Finally it is shown how the accuracy of the finite element values can be improved by the Richardson extrapolation7.
    Zusätzliches Material: 8 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080404
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  • 148
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    A few remarks on the paper: ‘Parameters of Gamma and Beta distribution’ (1974)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 8 (1974), S. 914-916 
    Details
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: The paper shows a procedure for estimating the shape parameter of a Gamma distribution from a sample. This procedure uses a rapidly converging iteration to solve the maximum-likelihood equation and suggests a simple formula for determing the starting value.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/nme.1620080416
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  • 149
    Digitale Medien
    Digitale Medien
    Identification of 2-hydroxy fatty acids in complex mixtures of fatty acid methyl esters by mass chromatographyAbbreviations: Hydroxy fatty acids are identified by h preceding chain length. (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 10-14 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Repetitive mass spectrometric scanning of gas-liquid chromatographic effuents at short (6 to 15 s) intervals, with a digital computer for data acquisition, reduction and display, allows plots (mass chromatograms) to be made of the intensities of specific ion fragments. Plotting of m/e values characteristic for certain classes of compounds and/or individual components reveals the location of constituents in the gas chromatogram. This technique was applied to the identification of trimethylsilyl derivatives of unsubstituted and 2-hydroxy fatty acid methyl esters in mixtures obtained from acid catalyzed methanolysis of cat brain galactocerebrosides. The plot of total ionization intensity vs scan number generated the gas-liquid chromatogram. Mass chromatograms of m/e 73 and [M - 59]+ gave the locations in the gas-liquid chromatogram of the hydroxy fatty acid derivatives, and mass chromatograms of m/e 74 and [M]+ located the unsubstituted fatty acid derivatives. Integrated ion intensities were used to determine the composition of the mixture of fatty acids.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010105
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  • 150
    Digitale Medien
    Digitale Medien
    The structural elucidation of polyene macrolide antibiotics by mass spectrometry. Nystatin, amphotericin B and pimaricin (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 20-28 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Complete mass spectra of the pertimethylsilylated derivatives of three high molecular weight polyene macrolide antibiotics are reported for the first time. The fragmentation pathways which are proposed have been corroborated by the stable isotope derivatives d9-TMS and d3-acetyl. Accurate mass measurements and metastable transitions confirm the proposed fragmentation mechanisms in the low mass range. Nystatin - the macrolide of highest molecular weight in this study - expels several TMSOH molecules and a TMS radical. Amphotericin B underwent extensive rearrangements preliminary to eliminating a series of TMSOH molecules. An apparent equilibrium between the keto and ketal forms of amphotericin B facilitated the rearrangements. Pimaricin fragmented in a manner parallel to that of the other two macrolides. The sugar portion of the molecules dominated the fragmentation in the low mass region in the spectra of all compounds. The transfer of a TMS group from the sugar amine to the glycosidic oxygen was observed when the amino sugar was eliminated from the intact molecule. The resulting sugar ion then expelled ammonia.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010107
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  • 151
    Digitale Medien
    Digitale Medien
    Sex-linked specificity of the hepatic metabolism of steroids in rats. Mass fragmentography as a method for the assay of hydrogenated metabolites of corticosterone in the liver (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 29-39 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: A method is described for the separation, identification and quantitation of endogenous hydrogenated metabolities of corticosterone in rat liver Corticosterone, 5α- and 5β-dihydrocorticosterone, 3α,11β,21-trihydroxy-5α-pregnane-3,20-dione, 3β,11β,21-trihydroxy-5α-pregnane-3,20-dione, 3α,11β,21-trihydroxy-5β-pregnane-3,20-dione, 3β,11β,21-trihydroxy-5α-pregnane-3,20-dione, 5α-pregnane-3α,11β,20α,21-tetrol, 5α-pregnane-3α,11β,20β,21-tetrol and 5α-pregnane-3β,11β,20β,21-tetrol are specifically quantitated in one analysis by mass fragmentography all as their O-methyloxime pertrimethylsilyl derivatives. A pronounced difference in the amounts of these nine metabolites between male and female adult rats was found, while in newborn rats only the two tetrahydro-compounds bearing a 5α-hydrogen were detected in both sexes. On the other hand 3α,11β,1 5α,21-tetrahydroxy-5α-pregnan-20-one was detected only in the adult female as its second prominent metabolite of corticosterone. Corticosterone metabolites being biochemical markers of the sex-linked differentiation of the hepatocytes, their mass fragmentographic assay is proposed as a tool for the quantitative analysis of this type of gene expression.
    Zusätzliches Material: 8 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010108
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  • 152
    Digitale Medien
    Digitale Medien
    Determination of the structure of partially methylated sugars as O-trimethylsilyl ethers by gas chromatography-mass spectrometry (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 62-65 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The separation and structural determination of ten partially methylated methyl glucosides by gas chromatography and gas chromatography-mass spectrometry are described. These glucosides were four possible structures for methyl tri-O-methylglucosides and six for methyl di-O-methylglucosides. The positions of free hydroxyl groups in four isomers of methyl tri-O-methylglucosides could be fairly distinguished from each other by their mass spectra. Mass spectra of methyl di-O-methylglucosides were similar to each other, though their spectra were different from those of fully methylated or methyl tri-O-methylglucosides. After introduction of a trimethylsilyl group to the free hydroxyl group, mass spectra of methyl di-O-methylglucosides showed a characteristic pattern for the position of the trimethylsilylated hydroxyl group, and O-trimethylsilyl ethers of methyl tri-O-methylglucosides also showed distinguishable mass spectra. The structures of fragment ions of partially methylated methyl glucosides were confirmed by high resolution mass spectrometry.
    Zusätzliches Material: 4 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010113
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  • 153
    Digitale Medien
    Digitale Medien
    Liquid chromatography-mass spectrometry. II - continuous monitoring (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 80-82 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Monitoring of solutes eluted from a liquid chromatograph is possible by continuous introduction of the effluent solution into the ion source of a chemical ionization mass spectrometer. Detection sensitivities in the nanogram range are possible for a wide variety of solutes and solvents. Auxiliary techniques which have proved valuable for g.c.-m.s. also appear to be applicable to l.c.m.s.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010117
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  • 154
    Digitale Medien
    Digitale Medien
    Study on drug metabolites by mass spectrometry. IVFor Part III, see Ref. 1. - metabolites of 2-(diethylamino) ethyltetrahydro-α-(1-naphthylmethyl)-2-furanpropionate oxalate in rats (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 66-72 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The determination of drug metabolites is very important in the biochemical field. However, the procedure for doing this has been very complicated in many cases. The major reason is because of the need for fairly large amounts of the samples. We have been studying procedures for the determination and identification by use of mass spectrometry, which usually gives a lot of information rapidly from very small amounts of the samples (below μg). In this paper, the metabolites excreted in urine and bile following oral administration of 2-(diethyamino)ethyl tetrahydro-α-(1-naphthylmethyl)-2-furanpropionate oxalate (1) in rats, were investigated by means of mass spectrometry and other techniques. The drug was not excreted unchanged in urine. Of the eight metabolites suspected to be present in urine and bile, the structures of three metabolites were elucidated to be tetrahydro-α-(1-naphthylmethyl)-2-furanpropionic acid (3) and α-(1-naphthylmethyl)-2-perhydro-5-oxofuranpropionic acid (4) in urine, and diethylaminoethanol (2) in bile. These metabolites might also be present as their structural isomers or conjugates.
    Zusätzliches Material: 11 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010114
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  • 155
    Digitale Medien
    Digitale Medien
    Masthead (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974) 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010201
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  • 156
    Digitale Medien
    Digitale Medien
    Interpretation of mass spectra, 2nd Edition, by F. W. McLafferty. W. A. Benjamin Inc., Reading, Massachusetts, 1973. $15.00 (cloth) $7.50 (paper) (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. xiv 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010118
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  • 157
    Digitale Medien
    Digitale Medien
    Qualitative and quantitative mass spectrometry of some noncatecholic biogenic amines and related compounds as their dansyl derivatives (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 83-95 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The use of the integrated ion current technique for the analysis of biogenic amines and phenols as their 1-dimethylaminonaphthalene-5-sulphonyl (dansyl) derivatives is described, particularly as regards to the linearity and sensitivity of detection. The mono derivatized amines gave a linear response over the range 10-9 to 10-14 mol, with a few being detected in quantities as small as 5 × 10-15 mol. The bisdansyl derivatives have a lower sensitivity and the response is linear over a more restricted range, terminating at 10-13 mol. Deuterated analogues of some of the amines were prepared and the feasibility of their use as internal standards was investigated. In this way, the problems associated with quantitative biochemical analyses caused by losses during extractions, chromatographic separations and thermal decomposition in the mass spectrometer lon source are overcome. The differentiation of isomers of biogenic amines as their dansyl derivatives has been accomplished by fractional sublimation and by examination of differences in their fragmentation patterns.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010202
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  • 158
    Digitale Medien
    Digitale Medien
    Amino acid mixture analysis by mass spectrometry in the form of their dimethylaminomethylene methyl esters (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 115-119 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The amino acids, arginine, citrulline, cysteine, cystine, histidine, hydroxyproline, methionine, ornithine, proline, serine, threonine, tryptophan and tyrosine, have been analysed in the form of their N-(N′, N′-dimethylaminomethylene) methyl esters. formed in a single step by reaction of the free amino acid or its hydrochloride with N,N-dimethylformamide dimethylacetal in acetonitrile/methanol (2:1). A reaction time of 15 minutes at 100 °C ensures complete derivatization, the derivatives being volatile at source temperatures below 150 °C, and giving electron impact spectra characterized by abundant (or moderately abundant) peaks at or near the mass of the molecular ion.The analysis of amino acid mixtures by mass fragmentography on characteristic high mass peaks of their N-(N′,N′-dimethylaminoethylene) methyl ester derivatives, introduced on a direct insertion probe and volatilized during temperature programming of the source, is qescribed. The method is applied to the analysis of a mixture containing arginine, citrulline, cystine, histidine and tryptophan, traditionally difficult to analyse by other methods.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010206
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  • 159
    Digitale Medien
    Digitale Medien
    Observations on the mechanism of hydroxylation of cyclophosphamide by rat liver microsomes: The metabolism of cyclophosphamide-4-d2 (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 130-136 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The metabolism of cyclophosphamide-4-d2 (2-[bis(2-chloroethyl)amino]-tetrahydro-4,4-dideuterio-2H-1,3,2-oxazaphosphorine 2-oxide), was studied. The first detectable metabolite was a hydroxy derivative which was trapped with ethanol. Mass spectrometry of the resulting two ethoxy derivatives and of the deuterated acrolein 2,4-dinitrophenylhydrazones formed therefrom via reaction with acidic 2,4-dinitrophenylhydrazine, afforded evidence that the ethoxy substituents were at C-4, which was therefore the position of the original hydroxy substituent. The mass spectrum of the deuterated acrolein 2,4-dinitrophenylhydrazone obtained from the total reactive metabolites was used to estimate the ratio of 4- to 6-hydroxylation. The rate of metabolism and the antitumour activity of cyclophosphamide and its 4-d2 analogue were compared.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010209
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  • 160
    Digitale Medien
    Digitale Medien
    Mass spectral studies of airborne particulates and possible pollution sourcesWork supported in part by EPA under Agreement No. EPA-IAG-0217(D) entitled ‘Correlation of Hazardous Compound Composition of Coal, Ash, Fly-Ash, and Other Emissions from Combustion’. (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 137-141 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The organic material in airborne particulate matter is being studied by high resolution mass spectrometry to determine if hydrocarbons typical of major sources of pollution can be detected. Carbon number distributions and hydrogen-to-carbon ratios of components found in airborne particulate samples and the corresponding data for compounds detected in fuel combustion products show great similarity. Samples collected near large power stations and major airports were compared with typical urban particulate samples. Particulates collected from jet engine exhaust and a condensate from the stack effluent from a coal-fired combustion system were studied. Mass spectral data were obtained for an auto exhaust tar, a coal tar pitch and several fuels. The mass spectra of two total particulate samples, compared to the spectrum of an ether extract of the organic matter, indicate that direct vaporization can be used and extraction is not essential for qualitative mass spectral studies.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010210
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  • 161
    Digitale Medien
    Digitale Medien
    Analysis of intact phospholipids by field desorption mass spectrometry (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 154-155 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The first application of field desorption mass spectrometry to the analysis of intact diacyl glycerophosphorylcholines (lecithins) has led to the detection of prominent molecular ions. This technique enables positive identification of the components of a mixture of phosphatidylcholines, which will provide valuable information on the phospholipid composition of biological fluids.
    Zusätzliches Material: 1 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010213
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  • 162
    Digitale Medien
    Digitale Medien
    Mass spectrometry of pesticides and pollutants, by S. Safe and O. Hutzinger. CRC Press Inc., Cleveland, Ohio, 1973. pp. 220, $32.00 (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 157-157 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010215
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  • 163
    Digitale Medien
    Digitale Medien
    News and events (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. xi 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010216
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  • 164
    Digitale Medien
    Digitale Medien
    Detection and quantitative analysis of amphetamine (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 159-162 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The high resolution mass spectrometric integrated ion current procedure has been used to identify and quantitate amphetamine, isolated as its dansyl derivative, as it is found after addition to urine and in tissues of the rat following intraperitoneal injection. A linear relationship between amphetamine and ion current response has been established at least in the range 5 × 10-12 to 5 × 10-7 g, and as little as 8 × 10-13 mol of amphetamine in urine may be detected.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010302
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  • 165
    Digitale Medien
    Digitale Medien
    Thin-layer chromatography-mass spectrometry for the identification of sapogenins from Digitalis species (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 166-168 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: A method is described for the identification of the sapogenins of several Digitalis species. The steroids are separated by repeated development thin-layer chromatography and identified by means of high resolution mass spectrometry. The spectra of tigogenin, gitogenin, digalogenin and digitogenin are recorded. These spectra are of particular use in establishing the position of extra hydroxy moieties in the steroid nuclei. Several species of Digitalis were screened for their sapogenin content. D. purpurea, D. mertonensis and D. lutea were found to contain tigogenin and digitogenin in small amounts, the principal steroid being gitogenin, whilst D. ambigua and D. lanata contained all four steroids.
    Zusätzliches Material: 2 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010304
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  • 166
    Digitale Medien
    Digitale Medien
    Intramolecular isotopic order in biologically produced acetic acid (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 172-174 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Acetic acid isolated from cider vinegar and inorganically synthesized glacial acetic acid have markedly different intramolecular isotopic distributions of the stable carbon isotopes. Carbon-12 is concentrated in the methyl group relative to the carboxyl group in the biologically produced acid. The reverse distribution is observed in the particular sample of glacial acetic acid examined here.
    Zusätzliches Material: 1 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010306
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  • 167
    Digitale Medien
    Digitale Medien
    Identification of some organic smog components based on rain water analysis (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 192-194 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: An analysis has been made of a sample of rain water collected in Washington, D.C. following a sustained photo-oxidant smog alert which was accompanied by haze and low visibility. The analysis was effected by purging the organic content from the water with helium gas and identifying the constituents by means of gas chromatography - mass spectrometry. The predominant compound was found to be 3-methylfuran, a possible intermediate or end product of the atmospheric decomposition of terpenoid hydrocarbons. The analysis suggests that the smog resulted from the air oxidation of hydrocarbons evolved from Appalachian forestation rather than from manassociated activities.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010309
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  • 168
    Digitale Medien
    Digitale Medien
    Source of the carboxamide nitrogen atom in 2-carboxamido-5-isopropoxycarbonylaminobenzimidazole, a metabolite of cambendazole (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 190-191 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Combined gas chromatography-mass spectrometry and isotope labeling techniques have been employed to demonstrate that the carboxamide nitrogen atom in 2-carboxamido-5-isopropoxycarbonylaminobenzimidazole, a metabolite of 2-thiazolyl-5-isopropoxycarbonylaminobenzimidazole (cambendazole), is derived wholly from the parent drug. [15N] Thiazole-labeled cambendazole was administered to a rat and the metabolite isolated from urine. Trideutero-2-carboxamido-5-isopropoxycarbonylaminobenzimidazole was employed as a carrier to isolate the metabolite in sufficient purity for isotope ratio measurements using multiple ion detection. The metabolite was converted to its tetramethyl derivative by on-column reaction with trimethylanilium hydroxide to permit satisfactory gas chromatography.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010308
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  • 169
    Digitale Medien
    Digitale Medien
    Workshop reports (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 206-207 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010312
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  • 170
    Digitale Medien
    Digitale Medien
    News and events (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. xiii 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010314
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  • 171
    Digitale Medien
    Digitale Medien
    Masthead (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974) 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010401
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  • 172
    Digitale Medien
    Digitale Medien
    Evaluation of bilirubin derivatives for mass spectral analysis (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 219-222 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Twelve derivatives of bilirubin were evaluated from the point of view of providing intense molecular ion peaks on electron impact and unambiguous molecular weights. The tetrakis-(trimethylsilyl) derivative of bilirubin was judged to be the most suitable because its molecular ion carries 22% of the total ion current and is the base peak in the spectrum. Molecular ions were found to carry 10% of the total ion current in the spectrum of the trimethylsilylated methyl ester of the phenylazo derivative of bilirubin. Fragmentation patterns of these two compounds were studied using deuterium labeling.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010404
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  • 173
    Digitale Medien
    Digitale Medien
    The use of Edman degradation in peptide mixture analysis by mass spectrometryA preliminary report including some of the data presented in this paper has been given at the 6th International Mass Spectrometry Conference, Edinburgh, Scotland, September 1973. (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 231-236 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Mass spectrometric analysis of peptide mixtures may lead to ambiguous results when it is possible to change from one peptide chain to another during the interpretation of the spectra. This kind of ambiguity can be eliminated by submission of part of the sample to one cycle of Edman degradation, followed by comparison of the results obtained for this preparation with those obtained for the nondegraded sample. Combination of this procedure with the use of deuterated derivatives has allowed an unambiguous interpretation for two mixtures of synthetic peptides.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010406
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  • 174
    Digitale Medien
    Digitale Medien
    Field desorption mass spectrometry of ten medicinal carbamates (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 256-262 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The field desorption mass spectra of ten medicinal carbamates - meprobamate, mebutamate, carisoprodol, emylcamate, bethanechol chloride, styramate, hydroxyphenamate, mephenesin carbamate, methocarbamol and chlorphenesin carbamate - were run and compared with their published electron impact spectra. Of the ten compounds run only emylcamate did not give a field desorption mass spectrum. All others gave abundant molecular ions, with the exception of bethanechol chloride which has a quarternary ammonium group and gave a field desorption spectrum characteristic of compounds possessing such a functional group. No general characteristic fragmentation was attributed to the carbamate function in the field desorption mode. However, the ease of obtaining abundant molecular ions or quasimolecular ions makes the field desorption method a valuable complementary technique to electron impact studies of carbamates.
    Zusätzliches Material: 9 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010409
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  • 175
    Digitale Medien
    Digitale Medien
    The determination of sequence information in homologously related proteins by mass spectrometry (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 269-273 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: An azurin, a small respiratory copper protein from the bacterium Pseudomonas fluorescens biotype G, has been studied by mass spectrometry to determine sequence information. The study of homologously related proteins by mass spectiometry is particularly attractive, since the correct nature of major parts of the deduced sequences can be confirmed by comparison with the sequences of the protein from related organisms. An oxidized tryptohan residue has been identified amongst the products from a cyanogen bromide digest of this wild type azurin. In the same digest, a product is also found to arise from cleavage of the peptide chain at the C-terminal side of the same tryptophan residue. These results are rationalized.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010411
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  • 176
    Digitale Medien
    Digitale Medien
    The mass spectral fragmentation of partially ethylated alditol acetates, a derivative used in determining the glycosly linkage composition of polysaccharidesSupported in part by AEC Contract No. AT(11-1)-1426.Abbreviations: PEGS = poly-(ethylene glycol succinate); PEGA = poly-(ethylene glycol adipate). (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 263-268 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The mass spectral data for the primary fragmentation of partially ethylated alditol acetates have been tabulated in order to allow easy reference for the identification of these polysaccharide derivatives. Sodium borodeuteride is used in all the aldose to alditol reductions, since the presence of a single deuterium label on C-1 greatly increases the information available in the mass spectrum and allows some identifications to be made which would not otherwise be possible. The primary fragmentations of these derivatives are analogous to those of the partially methylated alditol acetates, with each fragment shifted to a higher m/e value by fourteen mass units for each ether linkage contained in the fragment. The secondary fragmentation is also very similar, being characterized by the loss of acetic acid or ketene, or, less frequently, by the loss of ethanol or acetaldehyde. Coupled with the chromatographic retention time data for the partially ethylated alditol acetates tabulated elsewhere, the unambiguous mass spectral identification makes this derivative an excellent choice as a complementary derivative to the partially methylated alditol acetates for polysaccharide analysis. The utility of the partially ethylated alditol as a routine analytical derivative is further enhanced by the almost identical procedures required for synthesis of the ethyl and methyl derivatives. Through the combined use of these derivatives, most of the possible linkage isomers of the seven common aldoses of plant cell wall polysaccharides can be resolved, identified and quantitated.
    Zusätzliches Material: 2 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010410
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  • 177
    Digitale Medien
    Digitale Medien
    Characterization of cytosine nucleosides by mass spectrometry (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 281-285 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The mass spectra of most nucleosides of cytosine exhibit molecular ions of low abundance, rearranged ions base + 2H in greater abundance than the companion species base + H, and a characteristic and abundant ion which corresponds to base + C2HO from the sugar. Deuterium, oxygen-18 and substituent labeling showed the presence of C-1′, 2′, H-2′ and O-4′ in the latter ion, which led to a proposed mechanism of formation involving opening of the sugar ring and recyclization between O2 and C-2′ with expulsion of water. Primary driving force for the reaction is due to resonance stabilization promoted by unshared electrons from N4, which results in diminished abundance in the case of imino isomers and derivatives which contain electron-withdrawing groups at N4, and enhanced abundance resulting from methylation at N4. Data for 24 nucleosides are presented and discussed in terms of the determination of nucleoside structure.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010413
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  • 178
    Digitale Medien
    Digitale Medien
    News and events (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. ix 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010417
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  • 179
    Digitale Medien
    Digitale Medien
    Metabolism of branched medium chain length fatty acid: I - ω-oxidation of sodium dipropylacetate in ratsAbbreviations: DPA = dipropylacetate; BSA = N,O-bis-(trimethylsil)acetamide; TMCS = trimethylchlorosilane. (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 291-294 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The metabolism of sodium dipropylacetate (a newly developed anticonvulsant) was investigated in rats, and two metabolites were found in urine of rats which received dipropylacetate. The metabolites were identified as 2-n-propyl-5-hydroxypentanoic acid and 2-n-propylglutaric acid, respectively, by low and high resolution mass spectrometry. Synthetic 2-n-propylglutaric acid, when administered to rats, was not oxidized further and was excreted intact in urine. These data clearly show that ω-oxidation is involved in the metabolism of sodium dipropylacetate and that 2-n-propylglutaric acid, the end product of ω-oxidation, does not serve as a substrate for β-oxidation.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010415
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  • 180
    Digitale Medien
    Digitale Medien
    Limits of detection of carbon-13 labelled drugs and their metabolites in human urineAbbreviation used: PDB = Belemnitella americana (‘Peedee Belemnite’). (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 345-349 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The precise isotopic analysis of carbon by means of differential comparison of CO2 samples is applied to neutral, acid c and basic extract fractions of human urine. It is shown that the standard deviation of the analytical procedure, including sample preparation steps, is about 1% or 0.001 atom % excess carbon-13, but depends some what on the fraction considered. Day to day variations (expressed as standard deviations) in the isotopic composition of the urine fractions are generally less than 2.8%, 1.4% and 3.9% for the neutral, acidica and basic fractions, respectively, although the effect of unusual dietary inputs can be recognized. The ingestion of 23 μg excess carbon-13 in the form of isotopically labelled aspirin is shown to perturb significantly the isotopic composition of the acidic urine fraction which, for a 24 hour collection period, had a mass of 570 mg C. Because only 0.01% of the fraction was consumed by isotopic analysis, further extensive analysis would be possible. It is concluded that carbon-13 tracer experiments generally should be arranged to provide at least 5 × 10-5 g excess 13C/g carbon in any fraction which is to be used for lable detection.
    Zusätzliches Material: 4 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010510
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  • 181
    Digitale Medien
    Digitale Medien
    A method of analysis of dansylamides in mixtures by mass spectrometryAbbreviation: Dansyl = dimethylaminonaphthalene-5-sulphonyl. (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 363-364 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The mass spectra of a mixture twenty dansyl derivatives of biogenic amines were run using low energy electron impact. This method appears to be useful for the analysis of amines present in biological materials.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010514
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  • 182
    Digitale Medien
    Digitale Medien
    Masthead (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974) 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010601
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  • 183
    Digitale Medien
    Digitale Medien
    Mass spectrometric studies of thyroxine and related compounds. Trimethylsilyl derivatives (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 374-380 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The mass spectra of the trimethylsilyl derivatives of thyroxine and sixteen related compounds are reported. In addition to deiodinated analogues and iodinated tyrosines, the latter include a series of thyroacetic and thyropropionic acids and one thyroformic acid compound. Their spectra are discussed in terms of their fragmentation and utility for qualitative and quantitative estimation by gas chromatography - mass spectrometry.
    Zusätzliches Material: 2 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010603
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  • 184
    Digitale Medien
    Digitale Medien
    Mass spectrometry of the methyl ethers of isomeric hydroxychlorobiphenyls - potential metabolites of chlorobiphenyls (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 386-392 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The mass spectra of synthetic methoxychlorobiphenyls have been investigated. These substances are of interest as reference compounds in studies of the metabolism of chlorobiphenyls. Some characteristic fragmentation patterns have been found, useful for differentiation between the 2-, 3- and 4-methoxychlorobiphenyl isomers. Thus, mass spectra of 2-methoxychlorobiphenyls show large fragments at [M - CH3Cl]+., while those of 4-methoxy compounds differ from 3-methoxy isomers by the presence of significant [M - CH3]+ fragments in the former.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010605
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  • 185
    Digitale Medien
    Digitale Medien
    Identification of explosives by chemical ionization mass spectrometry using water as reagentAbbreviations: HMX (Octogen) = 1,3,5,7-tetranitro-1,3,5,7-tetrazacyclooctane; RDX (Hexogen, Cyclonite) = 1,3,5-Trinitro-1,3,5-triazacyclohexane; PETN = Pentaerythrytoltetranitrate. (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 393-396 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Chemical ionization mass spectra of four explosive compounds have been obtained by using water as reagent gas. The compounds are 1,3,5,7-tetranitro-1,3,5,7-tetrazacyclooctane, 1,3,5-trinitor-1,3,5-triazacyclohexane, pentaerythritol tetranitrate, and an explosive which has been used in letter bombs, containing the two latter compounds and a plasticizer. The chemical ionization H2O mass spectra were recorded at an ion source temperature range of 170 to 225°C, a probe temperature range of 160 to 265°C and a reagent gas (H2O) pressure range of 0.07 to 0.10 Torr. Unlike in chemical ionization using methane or isobutane, chemical ionization H2O spectrum of these compounds provides a method for obtaining quasimolecular peaks. Adduct ion peaks like [M + H3O]+, [M + H5O2]+, [M + NO]+ and [M + NO2]+ are also observed in the chemical ionization H2O mass spectra of these compounds. Chemical ionization H2O mass spectra provide thus a better means of explosive identification.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010606
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  • 186
    Digitale Medien
    Digitale Medien
    Carbon isotopic fractionations associated with acetic acid production by Acetobacter suboxydans (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 412-414 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Acetobacter suboxydans, strain 8.3, was grown using ethanol, made by the hydration of ethylene, as the sole energy source. After the microorganism had oxidized some of the ethanol to acetic acid, the unassimilated alcohol and produced acetic acid were isolated from the supernatant. Carbon isotopic analyses of these compounds and the starting ethanol show: (1) the methyl carbon of the starting alcohol is enriched in carbon-13 by 4.6% relative to the hydroxyl carbon, (2) the starting alcohol contains 2% less carbon-13 than the unassimilated ethanol and (3) the carboxyl carbon of the acetic acid excreted by the A. suboxydans is enriched by 3.8% in carbon-13 relative to the methyl carbon. These results support earlier findings which indicate that organisms preferentially utilize compounds enriched in carbon-12 and tend to concentrate carbon-12 in the reduced carbons relative to the oxidized carbons of metabolic products.
    Zusätzliches Material: 2 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010608
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  • 187
    Digitale Medien
    Digitale Medien
    Comparison of the field desorption, chemical ionization and electron impact mass spectra of some steroids (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 423-424 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The electron impact, chemical ionization and field desorption mass spectra of seven steroids showing varying stability to electron impact have been compared.
    Zusätzliches Material: 1 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010611
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  • 188
    Digitale Medien
    Digitale Medien
    Letter to the editors (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 427-428 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010613
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  • 189
    Digitale Medien
    Digitale Medien
    News (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. ix 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010615
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  • 190
    Digitale Medien
    Digitale Medien
    Mass spectra of compounds of biological interest, Volume 1 to 3, edited and compiled by S. P. Markey, W. G. Urban and S. P. Levine. USAEC TID-26553-P1, 2, 3. National Technical Information Service, U.S. Department of Commerce, Springfield, Virginia, 22161. 1974. pp. 1226. $28.80 (paper), $6.75 (microfiche) (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 428-428 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010614
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  • 191
    Digitale Medien
    Digitale Medien
    Masthead (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974) 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010101
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  • 192
    Digitale Medien
    Digitale Medien
    Editorial (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. xi 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010102
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  • 193
    Digitale Medien
    Digitale Medien
    Separation and characterization of isomeric substituted nucleosides by gas chromatography and mass spectrometryAbbreviations used: TMS (trimethylsilyl); TFA (trifluoroacetyl); TBDMS (t-butyldimethylsilyl). (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 78-79 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The 3′- and 5′-O-t-butyldimethylsilyl derivatives of thymidine and deoxyadenosine have characteristically different mass spectra and can be separated by gas chromatography.
    Zusätzliches Material: 1 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010116
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  • 194
    Digitale Medien
    Digitale Medien
    The collection and analysis of volatile hydrocarbon air pollutants using a timed elution chromatographic technique linked to a computer controlled mass spectrometer (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 73-77 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The difficulty of collecting volatile hydrocarbons, such as benzene, from street air in a form suitable for subsequent analysis is overcome by the use of a time-based elution procedure. By linking this technique to a gas chromatograph-mass spectrometer-data system, a rapid analysis is possible for low concentrations of collected material. Among advantages of this novel sample introduction procedure are the facility for collecting organic materials without interference from water vapour and their subsequent introduction into the g.c.-m.s. system without the use of any auxiliary solvents. Consequently the mass spectrometer can be used continuously on-line enabling the more volatile materials, normally masked by solvents, to be examined. This procedure is illustrated by the measurement of benzene and other hydrocarbon levels in street air (London). Following gas chromatographic separation the hydrocarbons can be identified by library search facilities attached to the mass spectrometer.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010115
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  • 195
    Digitale Medien
    Digitale Medien
    Forthcoming events (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. xiv 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010119
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  • 196
    Digitale Medien
    Digitale Medien
    News and events (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. xv 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010120
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  • 197
    Digitale Medien
    Digitale Medien
    Reagent gases for G.C.-M.S. analyses (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 96-102 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Several reagent gases and mixed reagent gases for high pressure ion-molecule reaction ionization of samples have been investigated for use in gas chromatography-mass spectrometry analyses. The common g.c. carrier gases and their mixtures with other gases such as isobutane, ammonia, tetramethylsilane, hexafluoroacetone and nitric oxide, were studied. These reagents were used to enhance the molecular ion intensity and to simplify the spectra of steroidal alcohols and the trimethylsilyl ethers of biologically important compounds.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010203
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  • 198
    Digitale Medien
    Digitale Medien
    Studies in organic mass spectrometry: XVSande, C. Van de; Vandewalle, M. Bull. Soc. Chim. Belges 1973, 82, 775. - mass fragmentographic identification of epinine in adrenal medulla and as a product of an in vitro enzymic methylation (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 103-108 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The presence of epinine in adrenal medulla and in reaction mixtures of enzymic in vitro experiments is proven by mass fragmentography. Derivatization of catecholamines, suitable for gas chromatographic analysis is discussed. The perfluoropropionates were selected for mass fragmentography.
    Zusätzliches Material: 8 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010204
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  • 199
    Digitale Medien
    Digitale Medien
    Mass spectrometry of 16,16′-O-permethylated 17-ketosteroidsAbbreviations used: A (androsterone); EA (epiandrosterone); E (etiocholanolone); DHA (dehydroandrosterone); DHEA (dehydroepiandrosterone); 11 OH-A (11 β-hydroxyandrosterone); 11 OH-E (11 β-hydroxyetiocholanolone). (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 109-114 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Using methylsulphinyl carbanion as base. methylation of 17-ketosteroids with methyl iodide not only converts hydroxy into methoxy groups, but also replaces both C-16 hydrogen atoms by methyl groups. These permethyl derivatives are very stable, have excellent properties for gas chromatographic separation and fragment characteristically upor electron impact. The mass spectra of a number of these derivatives are discussed.
    Zusätzliches Material: 11 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010205
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  • 200
    Digitale Medien
    Digitale Medien
    High resolution field desorption mass spectrometry: II - glycosides (1974)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1974), S. 120-123 
    Details
    ISSN: 1052-9306
    Schlagwort(e): Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The high resolution field desorption mass spectra of a number of glycosides are described. In all cases the spectra enabled molecular weights and elemental formulae to be established, and the presence of fragment ions due to cleavage of the sugar groups provides considerable assistance in the identification of sugar and aglycone moieties. The [M + 23Na]+ ion was the base peak in the spectrum of the sodium salt of testosterone glucuronide, and the presence [M + 39K]+, [M + 41K]+ and [M + 23Na]+ ions in the spectra of other glycosides are attributed to the presence of their sodium or potassium salts as impurities.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/bms.1200010207
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