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  • 1860-1869  (4,448)
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  • 1
    Electronic Resource
    Electronic Resource
    Springer
    Pflügers Archiv 401 (1984), S. 304-314 
    ISSN: 1432-2013
    Keywords: Visual cortex ; Contrast/response function ; Orientation and direction sensitivity ; Ocularity ; Binocular responses ; Feature specific responses ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Abstract The responses of neurons in area 17 were tested as a function of various stimulus parameters. The thresholds of individual cortical neurons were at contrasts between 0.01 and 0.1 (increment of 0.5×10−1 cd/m−2 on a background of 3 cd/m−2), the dynamic ranges were 1.0–2.0 log units of increment, and all cells showed a response decrease at increments above a certain maximum (supersaturation response). The averaged contrast/response curve for all neurons was S-shaped in the logarithmic plot, had a dynamic range of 2.5 log units, reached its maximum at a contrast of 0.75 and supersaturated above this level. The contrast/ sensitivity curves changed their slope under different stimulus conditions. They became flatter when the non-dominant eye was stimuated as compared to dominant eye stimulation or when the stimulation was done at a non-optimal orientation or direction, and they became steeper when both eyes were stimulated. But the maximum was reached at the same contrast and supersaturation was seen above maximum contrast no matter whether a cell was stronlgy (e.g. binocular stimulation at optimal orientation) or weakly excited (non-dominant or non-optimal orientation stimulation). After normalization, the averaged population contrast/response curves were virtually identical at all stimulus conditions. It was concluded, that range as well as maximum and supersaturation of cortical contrast/response curves are determined before the input reaches the cortex, and that the cortical cells summate, essentially, linearly. The findings furthermore demonstrate that the supersaturation of the cortical input must be due to subtractive inhibition, and that the same is true for the orientation sensitive inhibition in the cortex itself. Both, the peripheral contrast and the cortical orientation dependant inhibition cannot be explained by multiplicative inhibition. The fact, that the responses of neurons depend on many variables relativates their significance for feature representation.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Archives of toxicology 55 (1984), S. 178-181 
    ISSN: 1432-0738
    Keywords: Cat ; Phospholipids ; Acrylamide ; Neuropathy ; Lipids
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Abstract Treatment of cats with acrylamide, either 7.5 or 15 mg/kg IM, once a day for 10 days, resulted in increases of 31 and 47% in the phospholipid content of sciatic nerve, respectively, from a control level of 41.1±2.7 mg/kg wet weight. Determination of the distribution of individual phospholipids indicated no significant differences between control cats and those receiving a cumulative dose of 150 mg/kg acrylamide. In a separate experiment, cats were treated with the 150 mg/kg dose of acrylamide and the sciatic nerve was divided into proximal and distal portions at the level of the triceps surae nerve. Significant increases in phospholipid content were observed in both the proximal and distal portions of peripheral nerve of the acrylamide-intoxicated cats. This effect was present even when the phospholipid content was expressed in terms of total protein, dry weight or total lipid. Total weight of nerve segments, however, was significantly decreased in the neuropathic animals. The data are consistent with a focal degeneration of axons with relative sparing of phospholipids.
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Anatomy and embryology 170 (1984), S. 265-277 
    ISSN: 1432-0568
    Keywords: Midbrain ; Spinal cord ; Cat ; Degeneration-HRP
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The projections to the midbrain from the spinal cord have been investigated in the cat with the degeneration technique and by using horseradish peroxidase (HRP) as an anterograde tracer. Two types of spinal cord lesions were performed: 1) Cordotomies at cervical or thoracic levels transecting the ventral and lateral funiculi. 2) Transections of the ventral, ventrolateral, dorsolateral or dorsal funiculus, respectively, at cervical levels. In the anterograde tracing experiments HRP was injected into the spinal cord at cervical, lumbar or sacral levels. The results show large projections to the lateral and ventrolateral parts of the periaqueductal gray (PAG1), the posterior pretectal nucleus (PP) and the nucleus of Darkschewitsch (D). More moderate projections go to the medial division of the periaqueductal gray (PAGm), the cuneiform nucleus (CF), the mesencephalic reticular formation (MRF), lateral part of the deep layer of the superio colliculus (SP) and magnocellular medial geniculate nucleus (GMmc), while scattered spinal fibers are present in the dorsal part of the periaqueductal gray (PAGd), the external inferior collicular nucleus (IX), the intermediate layer of the superior colliculus (SI), the lateral part of the red nucleus (NR) and in the Edinger-Westphal portion of the oculomotor nucleus (3). In addition a few fibers are present in the interstitial nucleus of Cajal (CA) and anterior pretectal nucleus (PAc). The results indicate that at midcervical levels most of the spinomesencephalic fibers ascend in the ventral funiculus, with only a moderate fraction ascending in the ventral half of the lateral funiculus. Almost no fibers ascend in the dorso-lateral funiculus and none appear to pass in the dorsal funiculus. No distinct somatotopic pattern was found in the spinomesencephalic projections, but more fibers from cervicobrachial segments terminate in the rostral than in the caudal parts of the terminal fields in PAG, CF, SP and IX, while the lumbar fibers were more numberous in the caudal parts. PP seems to receive spinal fibers mainly from the caudal half of the cord.
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    Anatomy and embryology 170 (1984), S. 29-43 
    ISSN: 1432-0568
    Keywords: Anatomy ; Anterograde tracing ; Dorsal column nuclei ; Midbrain ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The termination of the fibers from the dorsal column nuclei (DCN) to the midbrain has been investigated in the cat with the degeneration method, the anterograde horseradish peroxidase (HRP) method and autoradiography after 3H-leucine injections. The results show that the DCN project to several midbrain regions. The external nucleus of the inferior colliculus (IX) receives the heaviest projection from both the gracile and cuneate nuclei. The DCN fibers form three joint terminal zones in IX. Each terminal zone contains clusters with dense aggregations of DCN fibers. Fairly dense terminal networks are found in the posterior pretectal nucleus (PP) and the compact part of the anterior pretectal nucleus (PAc) as well. More scattered DCN fibers are present in the cuneiform nucleus (CF), the lateral part of the periaqueductal gray (PAG1), the red nucleus (NR), the nucleus of the brachium of the inferior colliculus (B), the mesencephalic reticular formation (MRF) and the intermediate and deep layers of the superior colliculus (SI, SP). The projections to all regions are mainly contralateral. Most of the few ipsilateral fibers terminate in IX. A somatotopic organization was seen in IX and NR. The gracile fibers terminate preferentially in the caudal and lateral part of IX and the cuneate ones preferentially in its rostral and medial part. In the red nucleus the gracile fibers terminate ventral to the cuneate ones. In the pretectal region there was a predominance for gracile fibers. There also appeared to be quantitative differences in the projections from various levels of the gracile nucleus, with more midbrain projecting fibers originating in the rostral than in the middle and caudal parts of the nucleus.
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  • 5
    Electronic Resource
    Electronic Resource
    Springer
    Anatomy and embryology 170 (1984), S. 177-186 
    ISSN: 1432-0568
    Keywords: Cecum ; Cat ; Macroscopic anatomy ; Light, scanning and transmission electron microscopy
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary In a series of comparative anatomical studies on the ceca of various mammals the cat was chosen as representative of a “typical” carnivore. In the domestic cat, the cecum is conspicuously small and macroscopically relatively undifferentiated in comparison to most herbivores. Microscopically (light, scanning and transmission electron microscopy), however, it is characterized by an abundance of goblet cells and enterocytes rich in organelles, suggestive of functional activity. In addition to the morphological description, which also includes arterial supply and mesenteries of the cecum, the discussion is focussed on 1) the possible functional significance of the numerous goblet cells 2) a general categorization of the different types of ileal-caeco-colical junctions and 3) speculations concerning the justification for considering the carnivore cecum as being rudimentary.
    Type of Medium: Electronic Resource
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  • 6
    ISSN: 1432-0568
    Keywords: Placenta ; Fetal microvasculature ; Corrosion casts ; Scanning electron microscopy ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The fetal microvascular architecture of the feline near-term placenta was investigated using scanning electron micrographs of partially fractured corrosion casts from plastic-filled vessels. The findings were compared with those on corresponding semithin histological sections. The branches of both umbilical arteries and veins roughly follow a course parallel to the zonary girdle on the allantochorionic side of the feline placenta in an acute-angled pattern of ramifications. They join the double-layered capilary networks in the chorionic lamellae of the labyrinth, which generally exhibit a chorio-uterine orientation and are partially twirled. On the allantochorionic side of the labyrinth, these fetal capillary networks are “suspended” on the maternal stem-artery-system of the placenta; on the uterine side, they have peduncular or tuft-like endings of capillary loops and are flattened by the uterine septa, which at this level converge into the maternal veins. The chorionic capillary lamellae have a variable breadth and length and therefore need shorter or longer arterioles and venules from the allantochorionic side to become irrigated at any level of the labyrinth. As a result, the feline placenta is characterized by a generally one-way crosscurrent type of materno-fetal blood flow.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 95-106 
    ISSN: 1432-1106
    Keywords: Cerebellothalamic projections ; Pallidothalamic projections ; Ventral nuclei of thalamus ; Autoradiography ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Injections of 3H-leucine were made in the entopeduncular nucleus or dentate nucleus of the cerebellum in eight cats. The terminal projection zones of both pathways in the thalamus were studied using the sagittal plane and their relationships to one another as well as to cytoarchitectural boundaries of thalamic nuclei were compared. The data indicate that the territories controlled by the two projection systems are almost entirely segregated. The segregation is mainly along the antero-posterior axis as the main pallidal projection zone occupies the medio-ventral VA while the main dentate projection zone lies posterior to it in the VL. Furthermore, the dorsolateral part of the VA not occupied by pallidal projections receives dentate projections. In the VM, both afferent systems terminate in the lateral part of the nucleus with pallidal territory located anteriorly and dentate territory located posteriorly, again without overlap. As the delineations of nuclear subdivisions in the ventral thalamus of the cat have been a subject of some controversy, it is suggested that the boundaries of the VA, VL and VM in the cat thalamus be defined on the basis of basal ganglia and cerebellar projection zones.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 107-120 
    ISSN: 1432-1106
    Keywords: Corticospinal collaterals ; Sensorimotor cortex ; Corticobulbar pathways ; Fluorescent tracers ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The fluorescent retrograde double-labeling technique has been used to determine whether corticospinal neurons in the cat sensorimotor cortex distribute collaterals to the lower brain stem reticular formation. In this study the fluorescent tracers Nuclear Yellow and Diamidino Yellow 2HCl were used in combination with Fast Blue. One tracer was injected unilaterally in the spinal cord and the other was injected ipsilaterally in the bulbar medial reticular formation. The distribution of the retrogradely labeled neurons was studied in the contralateral hemisphere. In the sensorimotor cortex a large population of neurons was found which were labeled from the spinal cord and were double-labeled from the brain stem. These branching neurons were concentrated in the rostromedial part of area 4 and the adjoining lateral part of area 6. In this region the percentages of corticospinal neurons which were double-labeled from the brain stem ranged from 5% laterally to 30% medially. In two cats it was demonstrated by means of the anterograde transport of HRP that the corticobulbar fibers from this region which must include the corticospinal collaterals are distributed to the reticular formation of the lower brain stem. In view of the fact that the double-labeled neurons are concentrated in the anterior part of the motor cortex, those branching neurons are in all likelihood involved in the control of neck, back and shoulder movements. This control is probably exerted by way of two routes i.e. by way of the direct corticospinal connections to spinal interneurons, and by way of the indirect cortico-reticulospinal connections established by the cortical fibers to the bulbar reticular formation. The present findings suggest that this dual control may be exerted by one and the same cell.
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  • 9
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 203-211 
    ISSN: 1432-1106
    Keywords: Ascending auditory pathway ; Inferior colliculus ; Medial geniculate body ; Cat ; Autoradiography
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Ascending projections from the nucleus of the brachium of the inferior colliculus (NBIC) in the cat were studied by the autoradiographic tracing method. Many fibers from the NBIC ascend ipsilaterally in the lateral tegmentum along the medial border of the brachium of the inferior colliculus. At midbrain levels, fibers from the NBIC end in the superior colliculus, the pretectum, the central gray and the peripeduncular tegmental region bilaterally with ipsilateral predominance. NBIC fibers to the superior colliculus are distributed densely to laminae VI an III throughout the whole rostrocaudal extent of the colliculus. In the pretectum, NBIC fibers terminate in the anterior and medial nuclei and the nucleus of the posterior commissure. NBIC fibers to the dorsal thalamus are distributed largely ipsilaterally. Many NBIC fibers end in the dorsal and medial divisions of the medial geniculate body, but few in the ventral division. The NBIC also sends fibers to the suprageniculate, limitans and lateralis posterior nuclei and the lateral portion of the posterior nuclear complex; these regions of termination of NBIC fibers constitute, as a whole, a single NBIC recipient sector. Additionally, the NBIC sends fibers to the centralis lateralis, medialis dorsalis, paraventricular and subparafascicular nuclei of the thalamus.
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  • 10
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 395-405 
    ISSN: 1432-1106
    Keywords: Neonatal ; Bilabyrinthectomy ; Recovery ; Locomotion ; Vision ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Four cats labyrinthectomized shortly after birth (DELAB) exhibited the classical vestibular syndrome and recovery, while their motor development was otherwise unimpaired. As adults, they were tested for visual vestibular substitution in a locomotor task with either orientation requirements (tilted platforms) or balance requirements (narrow platforms). Visual motion cues or static visual cues were controlled using normal or stroboscopic lighting, or darkness. Measurements of the average speed of locomotion showed that: Although all cats increase their speed when more visual cues become available, a marked deficit occurs in darkness only in the DELAB cats. With either vestibular cues alone or static visual cues alone, cats are able to reach the same level of performance in the tilted platform test, which suggests a total visual-vestibular interchangeability in orientation. DELAB cats perform very poorly in the narrow rail test. When continuous vision is allowed in the narrow rail test the DELABs' performance rises but does not match that of the control group. A specific deficit in balance for the DELAB group is thus reduced by normal continuous vision as compared to stroboscopic vision, suggesting a significant, though imperfect, substitution of motion visual cues for the missing dynamic vestibular cues. Dynamic visual cues play only a minor role in most situations, when locomotory speed is high. This results support the view that both the vestibular and the visual system can subserve two distinct functions: dynamic information may stabilize the stance in narrow unstable situations, during slow locomotion. and static orientation cues may mainly control the direction for displacement. Possible interactions between head positioning and body orientation in the DELAB cats are discussed.
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  • 11
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 377-381 
    ISSN: 1432-1106
    Keywords: Pupillo-constrictor areas ; Afferents ; HRP ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Afferents of the cortical pupillo-constrictor areas (PCAs) of the cat were studied using the horseradish peroxidase method. PCAs receive heavy cortical inputs from areas 7, 19, 21, the lateral suprasylvian area, the splenial visual area, and subcortically from the claustrum, the intralaminar nuclei, the pulvinar-lateral posterior nuclear complex.
    Type of Medium: Electronic Resource
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  • 12
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 253-258 
    ISSN: 1432-1106
    Keywords: Lateral geniculate nucleus ; Pretectal nuclei ; Superior colliculus ; Parabigeminal nucleus ; Reticular formation ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The ascending connections from the brainstem to the dorsal division of the lateral geniculate nucleus were examined using retrograde transport of horseradish peroxidase. Labelled cells were identified in a variety of structures, including the nucleus of the optic tract (NOT), the posterior pretectal nucleus (NPP), the superior colliculus (SC), the parabigeminal nucleus (PBN), the midbrain reticular formation (MRF), locus coeruleus and nucleus sub-coeruleus, the substantia nigra (SN), and parts of the raphe complex. The projections from NOT, NPP, MRF, LC and PBN were all bilateral in origin. The most intense labelling was observed in the nucleus of the optic tract and the superior colliculus. Colliculo-geniculate cells were located primarily in the superficial gray lamina II1 and II2 of Kaneseki and Sprague (1974), but sparse labelling was also observed in lamina II3 and in statum opticum (lamina III). Consistent with the report of Harrell et al. (1982), these cells represent a morphologically diverse population, which includes stellate cells, granule cells, and both vertical and horizontal fusiform cells. A similarly diverse population of cell types contributes to the geniculate projection arising from NOT. These results confirm and extend earlier descriptions of the brainstem projections to the cat LGNd, and serve to emphasize the diversity of brainstem influences over the geniculate.
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  • 13
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 55 (1984), S. 134-144 
    ISSN: 1432-1106
    Keywords: Cat ; Tracking ; Isometric ; Updating ; Delayed feedback
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary 1. In cats trained to track a moving display by making rapid, isometric force adjustments, responses are characterized by extremely short reaction times (60–70 ms) and a stereotyped temporal configuration. The animal uses early derivatives of display movement to scale force responses to target stimuli of different sizes according to a learned relationship between initial display motion and required force (Ghez and Vicario 1978a, 1978b). In the present study we altered that relationship by using double stimulation and delayed feedback to assess the animals' ability to update their responses. 2. In experiments where a second target stimulus followed the first after a controlled interval (15–120 ms) on random trials, the animal modified its response in the appropriate direction with little or no increase in reaction time. When the second stimulus called for a return to baseline, the animal aborted the ongoing response. When the second stimulus called for a doubling of force, the animal increased its phasic force output; however, this increase was not sufficient to reach the new target level and late responses were emitted. 3. The control response which followed each experimental double stimulation trial showed consistent differences from other controls in the amplitude of both peak force and peak dF/dt. Control responses following trials calling for a return were reduced in size; those following stimuli requiring response doubling were increased. We concluded that the experimental trials not only elicited modification of ongoing responses but also caused the animal to alter its internalized gain function relating initial display derivatives to required force. 4. In experiments where feedback was delayed after giving a first target stimulus such that the compensatory display failed to reflect the animal's initial response, the animal emitted a new updated response 70–80 ms after the first. The display trajectory which caused the cat to update its response on delayed feedback trial was identical to that of control trials with long reaction times. In this case, however, the information eliciting response updating had to be derived as a difference between the actual display trajectory and that expected by the animal, based on its experience with the tracking task. This suggests that the animal develops an internal model of display properties which is used to determine when a new response is required.
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  • 14
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 55 (1984), S. 152-157 
    ISSN: 1432-1106
    Keywords: Deafferentation ; Cross reinnervation ; Contractile properties ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Cross-reinnervations were effected between the extensor digitorum longus and soleus muscles in the cat hind limb. At the same time dorsal root section or ganglionectomy was performed over segments L6-S1. Completeness of the deafferentation was subsequently confirmed either by dissection or by dorsal root recording. The isometric and forcevelocity properties of the muscles were measured. In animals with a unilateral cross plus deafferentation the conversion of the contractile properties of the normally slow-twitch soleus to those resembling a fast-twitch muscle was typical of that seen with an intact afferent supply. In cats with a bilateral cross-reinnervation and unilateral deafferentation there was no significant difference in the degree of transformation between the two sides. It is concluded that at least for the conversion of a slow-twitch to a fast-twitch muscle afferent feedback does not play a major role.
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  • 15
    ISSN: 1432-1106
    Keywords: Optic nerve section ; Cat ; Pattern ERG ; Retinal morphology
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Previous experiments have shown that the ERG response to alternating gratings vanishes gradually within 4 months after transection of the optic nerve, changes begin after 2–3 weeks. The response to gratings of low spatial frequencies deteriorates earlier than the response to gratings of high spatial frequencies (Maffei and Fiorentini 1981). Quantitative analysis of ganglion cell sizes in retinal wholemounts shows that ganglion cell shrinkage and ganglion cell loss begin at three weeks in the periphery of the retina, particularly in the temporal retina. The same morphological alteration subsequently becomes apparent also in the area centralis and the nasal retina, respectively. The main and early cell loss occurs among medium sized ganglion cells, supposedly the beta-cells. Among the alpha-cells only shrinkage is observed up to two months postoperatively. Light- and electron microscopic examination of cross sections through the retina show that pathological changes are restricted to the innermost layers.
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  • 16
    ISSN: 1432-1106
    Keywords: Glutamatergic synapses ; Vestibular nerve lesion ; Vestibular nuclei ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Evidence that glutamate acts as a neuro-transmitter in vestibular nerve fibers was sought (1) by electron microscope radioautographic identification of the uptake sites of [3H]-glutamic acid after incubation of slices of cat vestibular nuclei, and (2) by measuring changes in sodium-dependent high affinity glutamate uptake in nerve endings containing homogenates from normal and deafferented vestibular nuclei 8 to 11 days after unilateral vestibular nerve lesion. Electron microscopic radioautography revealed that glutamate had been taken up by numerous nerve endings projecting over the whole vestibular nuclear complex. The biochemical approach indicated that after section of the vestibular nerve, a significant decrease in high affinity glutamate uptake occurred in the vestibular nuclei, which lost their exclusively ipsilateral projection. This decrease varied from one area of the deafferented vestibular nuclei to another, reaching −58% in the lateral area of the central part corresponding to the ventral lateral vestibular nucleus and the rostral part of the descending vestibular nucleus. It is concluded that glutamate (or aspartate) is used by the vestibular nerve fibers as a neurotransmitter in the vestibular nuclei.
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  • 17
    ISSN: 1432-1106
    Keywords: Corticocortical connections ; Motor cortex ; Areas 4, 5a, 5b, 7 ; Posterior parietal lobe ; Retrograde transport of HRP ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Neurons in the parietal region of the cerebral cortex, projecting to the ipsilateral distal forelimb area of the motor cortex (area 4γ) were identified in the cat brain using the horseradish peroxidase (HRP) retrograde tracing method. After making microinjections of HRP into the distal forelimb area of the motor cortex, clusters of HRP-labeled cell bodies were observed in different regions of the ipsilateral parietal cortex. In particular these clusters of labeled cells were found in areas 5a, 5b and 7. The area 5a cluster is formed from closely packed irregularly-shaped cells, the area 5b cluster is made up of dispersed medium-sized pyramidal cells, while area 7 contains a cluster of widely dispersed small pyramidal cells. Typically, labeled cell bodies were found in lamina III of cortex. Labeled cell bodies were neither observed in the contralateral cortex nor in the visual cortex (areas 17, 18 and 19). Since parietal cortex receives projections from primary somatosensory and visual cortex, the projections from parietal to motor cortex may well form the neural substrate for the processing of convergent sensory information used in voluntary movements.
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  • 18
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    Electronic Resource
    Springer
    Experimental brain research 56 (1984), S. 162-166 
    ISSN: 1432-1106
    Keywords: Vestibular nerve afferents ; Semicircular canal biophysics ; Semicircular canal time constants ; Vestibular neurophysiology ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The response properties of cat horizontal canal afferents (N = 81) were characterized by three parameters: their long time constants (τ), low frequency gain constants (G1), and middle frequency gain constants (Gm). An average value of each of these parameters was calculated for each of eight animals and comparisons were made across animals. There were significant differences between individual animals in their average values of τ and Gm. There was also a significant negative correlation between τ's and Gm's. An animal with a larger average τ tended to have a smaller average Gm. We also used anatomic data on membranous canal duct diameter from the literature to independently estimate the potential effect of interanimal anatomic variability on the predicted range of τ and Gm values in a population. We then compared the data from our 81 afferents with the predictions from the anatomic data.
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  • 19
    Electronic Resource
    Electronic Resource
    Springer
    Experimental brain research 53 (1984), S. 259-276 
    ISSN: 1432-1106
    Keywords: Motor cortex ; Thalamocortical ; Corticocortical ; HRP ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary (1) Ipsilateral cortico-cortical and thalamo-cortical projections to the cat motor cortex were determined from the locations of retrogradely labeled neurons following single small intracortical injections of HRP in area 4γ. These projections were also examined by studying the distribution of anterogradely transported axonal label following multiple injections of HRP or of tritiated amino acids in areas 1–2 of SI and in area 2pri (SII). (2) The number of retrogradely labeled cells in areas 1–2 and in area 2pri differed markedly between HRP injection sites located in the precruciate (anterior sigmoid gyrus) and postcruciate (posterior sigmoid gyrus) subregions of area 4γ. These associational projections from primary and secondary somatosensory cortices were dense to postcruciate subrogions but weak to the precruciate subregions. (3) The associational projections from areas 1–2 and from area 2pri to the postcruciate subregion of area 4γ were topographically organized, but no clear topographic organization could be demonstrated for the precruciate projection. (4) Anterograde terminal labeling following injection of either HRP or tritiated amino acids into areas 1–2 and area 2pri confirmed the preferential projection of somatosensory cortex to the postcruciate subregion of motor cortex. The projection from somatosensory areas 1–2 was uniform over its terminal field, but that from area 2pri was more patchy and complex. (5) HRP injections in area 4γ gave rise to lamellae of labeled neurons in the ventrolateral nucleus of thalamus (VL). A topographic relationship was found between the site of injection and the location of the lamella of labeled neurons. (6) The percentage of retrogradely labeled neurons in the shell zone surrounding the border of the ventrolateral nucleus and the ventrobasal complex (VB) was greater following postcruciate than precruciate injections, whereas fewer retrogradely labeled neurons were found in central lateral nucleus (CL) after postcruciate injections than after precruciate injections. (7) These observations support the hypothesis that differential cortical and thalamic projections to different subregions of area 4γ may give rise to the different physiological properties of neurons observed in these subregions (Vicario et al. 1983; Martin et al. 1981).
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  • 20
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    Electronic Resource
    Springer
    Experimental brain research 54 (1984), S. 283-288 
    ISSN: 1432-1106
    Keywords: Skin potential response ; Cat ; Pyramidal tract ; Reticulospinal tracts
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Pyramidal command of Skin Potential Response (SPR) was investigated in 20 cats paralyzed by gallamine and under a halothane anaesthetic. For each animal, a transection of the medulla sparing only the pyramidal tract was carried out. The pyramidal tract and Mesencephalic Reticular Formation (MRF) were stimulated before and after the transection. Results taken before transection show that the SPR can be elicited from stimulation of the pyramidal tract and the MRF. After transection, stereotaxic stimulations of the pyramidal tract still evoked the SPR even after aspiration of the medullary tissue posterior to the section and overlying the pyramids. Control reticular stimulations with higher stimulus intensities failed to evoke the SPR. These results show that stimulation of the pyramidal tract can elicit the SPR independently of reticulospinal neurons. It is hypothesized that a group of corticospinal fibers could transmit volleys having autonomic activity on preganglionic autonomic neurons of the intermediate zone of the grey matter.
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  • 21
    ISSN: 1432-1106
    Keywords: Central cervical nucleus ; Spinocerebellar tract ; Neck muscle afferents ; Spinal cord ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Extracellular and intracellular recordings were made from spinocerebellar tract neurones of the central cervical nucleus (CCN) in C1–C3 segments of the anaesthetized cat. These neurones were identified by antidromic activation from the cerebellar peduncle. Stimulation of the ipsilateral dorsal root elicited extracellular spikes or EPSPs with a monosynaptic latency in almost all CCN neurones in the same segment (segmental input). Late excitatory effects were also observed in about one third of CCN neurones. The monosynaptic EPSP was occasionally followed by an IPSP. The excitatory input from the dorsal root to CCN neurones was extended over several segments for some CCN neurons (extrasegmental input). Monosynaptic excitation was evoked in CCN neurones after stimulation of dorsal neck muscle nerves as well; i.e. splenius (SPL), biventer cervicis and complexus (BCC), rectus capitus dorsalis, and obliquus capitus caudalis. Thresholds for this excitation were near the threshold of the nerve, suggesting that it originated from group I fibres. The component of excitation added after strong stimulation of neck muscle nerves would be attributed to group II fibres. When a CCN neurone received excitatory input from the nerve of one muscle, it was generally not affected by stimulation of other nerves in the same segment. Such muscle specificity of segmental input was the principal pattern of connexion of neck muscle afferents with CCN neurones. In some cases, however, excitatory convergence from SPL and BCC nerves onto single CCN neurones or excitation from the SPL nerve and inhibition from the BCC nerve were also observed. Nearly half of the CCN neurones received input from one muscle nerve of the same segment and not from the afferent of the same muscle of different segments, indicating a segment specificity of input. In the remaining CCN neurones, weaker excitatory effects were induced from afferents of different segments as well. In such extrasegmental effects, inputs to CCN neurones from caudal segments predominated in frequency over those from rostral segments. The origin of extrasegmental input was generally confined to the same muscle. Low threshold muscle afferents from the SPL and BCC were intraaxonally stained with HRP. The collaterals of the stained fibre distributed branchlets and terminals to the CCN, laminae VII, VIII, and motor nuclei. Two fibres responding to local muscle prodding or stretch showed a similar morphology. The findings indicated that muscle spindle afferents from primary endings projected to the CCN.
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  • 22
    ISSN: 1432-1106
    Keywords: Central cervical nucleus ; Spinocerebellar tract ; Cerebellum ; Spinal cord ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Spinocerebellar tract (SCT) neurones in and around the central cervical nucleus (CCN) were physiologically identified by antidromic activation of these cells on stimulation of the cerebellum. Among the Spinocerebellar tract cells thus identified, those ascending the contralateral spinal funiculi were found in the CCN and ventralwards, whereas those ascending the ipsilateral funiculi existed mostly dorsal to the CCN partly overlapping with crossed cells in the nucleus. Mapping sites from which CCN cells were antidromically activated showed that axons of the CCN-SCT cross at the same segment, ascend the ventral funiculus initially, the lateral funiculus at rostral C1 and the lateral border of the medulla to reach the cerebellar peduncle, enter the cerebellum mainly via the restiform body but possibly also via the superior peduncle. Systematic mapping of stimulation within the cerebellum indicated that the CCNSCT projects to the medial part of the anterior lobe and the posterior lobe bilaterally. Projection to lobules I–II was found in almost all CCN-SCT cells examined. Three fourths of CCN-SCT cells projected to the posterior lobe, as revealed by less extensive mapping. Mapping of axonal regions of the same single CCN-SCT cells showed that they project multifocally in the cerebellum, where projection to lobules I–II was common and that to other areas varied with individual cells. Conduction velocites decreased within the cerebellum probably as the result of repeated branching. Mossy fibre responses evoked on stimulation of the C2 dorsal root in cats with the transected dorsal funiculi were shown to be mediated mostly via the CCN-SCT. Mapping the field potential showed that the response was by far the largest in lobules I–II. This suggested that the terminals provided by the CCN-SCT are the densest in these lobules.
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  • 23
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    Experimental brain research 55 (1984), S. 325-332 
    ISSN: 1432-1106
    Keywords: Endogenous peroxidase ; Light and electron microscopy ; Spinal cord ; Dorsal column nuclei ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Endogenous peroxidase-like activity was investigated with a combined light and electron microscopical technique in 15 cats. The lateral cervical nucleus, the dorsal column nuclei, and segments C6 and L5 of the spinal cord were incubated with diaminobenzidine-tetrahydrochloride (DAB) or tetramethylbenzidine (TMB). After histochemical reaction with DAB a considerable amount of activity was found in nerve cells, astrocytes and pericytes. The neuronal labelling was mainly located in mitochondria of axon terminals and in dendrites whereas the astrocytic and pericytic activity was found in cytoplasmic dense bodies. The quantity of stained structures differed considerably between the animals. In TMB reacted tissue endogenous peroxidase-like activity was only sparsely seen. It was found mainly in frozen sections, in which the neuropil and perivascular structures sometimes contained granules and irregular filaments. The significance of the findings is discussed in relation to observations in tracer studies using horseradish peroxidase.
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  • 24
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    Experimental brain research 55 (1984), S. 470-482 
    ISSN: 1432-1106
    Keywords: Congenital microstrabismus ; Cat ; Visual cortex ; Binocularity ; Visual axis
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Twenty-nine pigmented offspring of an innately esotropic female cat exhibited varying deficits in the number of binocular cells recorded in area 17 of the visual cortex as compared to 12 normal cats. Misalignment of the two eyes in these cats was found in the awake as well as in the paralysed state. Pupillography combined with measurements of visual disparity yielded abnormal esotropia of up to 8.4° under paralysis, which corresponds to an abnormal convergence of the freely moving eyes of up to 14° (average 7.4°). In the majority of animals cortical binocularity was found reduced by the two eyes controlling independent sets of separate units (U-shaped ocular dominance distribution) whereas in 7 cats the reduction was due to a partial loss of one eye's influence. The proportion of monocular units correlated with the degree of crossover of the visual axes (r = 0.73). Anatomical investigation of the retinofugal projections revealed normal appearance in three previously recorded cats in which more than 50% of cortical units had been monocularly driven. The small angles of esotropia and the “normal” appearance of eye position judged by the pupillary positions in the orbit of these cats, might suggest that we found an animal model for microstrabismus.
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  • 25
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    Experimental brain research 55 (1984), S. 197-204 
    ISSN: 1432-1106
    Keywords: Phrenic and laryngeal motoneurones ; Inspiratory on-switch ; Stimulation ; Mesencephalic structures ; Patterned response ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary In anaesthetized cats (chloralose-urethan) the effects of brief tetanic electrical stimulation (50 to 100 ms) of the mesencephalic central gray matter and reticular formation on the inspiratory on-switch were studied during the expiratory (E) phase on the gross and unitary activities of phrenic, laryngeal inspiratory and laryngeal expiratory nerves. On the inspiratory laryngeal and phrenic nerves, stimulation elicited a short latency gross response concomitant with the train: the inspiratory Primary Response (Prim.R.) which is followed by an inspiratory Patterned Response (Patt.R.) of longer duration which corresponded to the inspiratory on-switch. The Patt.R. generally appeared from the Prim.R. within a latent period (Silent Phase: Sil.P.) as long as 100 ms. On the expiratory laryngeal nerve, stimulation elicited a brief activation (expiratory Prim.R.) concomitant with the beginning of the inspiratory laryngeal Prim.R. and which rapidly stopped as the latter continued during the stimulus train. The inspiratory Prim.R. corresponded to a simultaneous activation of both early and late (so defined during their spontaneous discharge) inspiratory motoneurones. The laryngeal motoneurones were more strongly activated than the phrenic ones. During the inspiratory Patt.R. all the phrenic motoneurones presented a recruitment delay earlier, compared with the spontaneous one, whereas the recruitment drastically changed from an inspiratory laryngeal motoneurone to another. Thus, the two pools of motoneurones presented different properties of activation. During the inspiratory Sil.P. no concomitant expiratory laryngeal activation was observed when most of the inspiratory motoneurones were inactive. As some inspiratory laryngeal motoneurones did not stop firing, the existence of some central respiratory neurones exhibiting a similar persistent activity and subserving the inspiratory on-switch mechanisms may be hypothesized.
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  • 26
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    Experimental brain research 56 (1984), S. 458-467 
    ISSN: 1432-1106
    Keywords: Cat ; Postnatal development ; Phrenic motoneurones ; Intercostal motoneurones ; Horseradish peroxidase
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The localization and morphology of spinal respiratory motoneurones (phrenic and intercostal) were studied in the cat by retrograde labelling using Horseradish Peroxidase (HRP), at different stages of postnatal development. At birth, the distribution of the phrenic and intercostal motoneurones in the cervical and thoracic ventral horn, respectively, is similar to that observed in adult animals. At birth, the phrenic and intercartilaginous motoneurone somata have respectively 60% and 40% of their adult volume, appearing much more developed than the motoneurones involved in the motor control of limbs. During postnatal development, the phrenic and intercartilaginous motoneurones undergo a characteristic sagittal elongation without evident modification along their transverse axes. From birth, the ratio of the somatic volume to that of its corresponding motor column markedly decreases inside of the phrenic column compared to the data obtained in the limb's muscle motor columns by other authors. Similar determinations in intercostal motor columns give intermediate values between those obtained from the phrenic column and from the motor system. These results indicate that the motoneurones innervating the respiratory muscles have some specific features of development.
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  • 27
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    Experimental brain research 53 (1984), S. 462-466 
    ISSN: 1432-1106
    Keywords: Visual cortex ; Contralateral connections ; Thalamus ; Cat ; Sub-cortical commissures
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Contralateral corticofugal projections from visual cortical areas to thalamic nuclei were demonstrated in the cat using anterograde transport of tritiated proline. Thalamic nuclei receiving projections from contralateral visual cortex include both subdivisions of the lateral-posterior nucleus, the posterior nucleus of Rioch, and the posterior nuclear complex.
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  • 28
    ISSN: 1432-1106
    Keywords: Spinal cord ; Scratch reflex ; Ventral spino-cerebellar tract ; Spino-reticulo-cerebellar pathway ; Cerebellum ; Cooling the nervous tissue ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary (1) The “fictitious” scratch reflex was evoked in decerebrate curarized cats by pinna stimulation. Activity of neurons of the ventral spinocerebellar tract (VSCT) from the L4 and L5 segments of the spinal cord as well as of neurons of the spinoreticulo-cerebellar pathway (SRCP) from the lateral reticular nucleus of the medulla oblongata was recorded. Cooling and destruction of different parts of the lumbo-sacral enlargement of the spinal cord were performed. (2) Cooling of the L5 or L6 segment abolished the rhythmic activity in the greater part of the spinal hindlimb centre but did not affect the generation of rhythmic oscillations in the remaining (rostral) segments of the lumbo-sacral enlargement. Under these conditions, neither the rhythmic activity of VSCT neurons located rostral to the thermode nor that of SRCP neurons changed. (3) A normal rhythmic activity of SRCP neurons also persisted after destruction of grey matter in the L3 and L4 segments. It can be concluded that activity of these neurons is independent of whichever part of the enlargement generates rhythmic oscillations. (4) From these observations a hypothesis is advanced that the main content of signals conveyed by the VSCT and SRCP to the cerebellum is the information regarding activity of the generator of rhythmic oscillations that is located in the L3-L5 spinal segments.
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  • 29
    ISSN: 1432-1106
    Keywords: Cat ; Rat ; Spinal tract neurons ; Retrograde HRP transport ; Procedure and evaluation
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Modifications have been made in Mesulam's method for labelling neurons by retrograde transport of horseradish peroxidase, with tetramethylbenzidine as chromogen, with the object of increasing the extent of labelling of dendrites and axons. A procedure was devised specifically for studying spinomedullary and medullospinal tract systems, involving implanting easily-made HRP-agar pellets into areas of controlled damage in particular spinal fascicles, and sealing the site of implant with cyanoacrylate glue. Lesions of other fascicles were often made to limit transport to the implanted fascicle. Fourth-order dendrites were regularly labelled over long (30 cm or more) transport distances: axons were also labelled over this whole distance, often allowing exact study of the initial course of particular axons. Controls in both cat and rat showed that the uptake of HRP under these circumstances occurred almost wholly from the region of axonal damage at the site of implant which can be characterized histologically.
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  • 30
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    Experimental brain research 55 (1984), S. 49-59 
    ISSN: 1432-1106
    Keywords: Accessory optic system ; Vestibulo ocular reflex ; Optokinetic nystagmus ; Cat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary Horizontal vestibulo-ocular reflex (VOR) and optokinetic nystagmus (OKN) were studied before and after lesions within the accessory optic system (AOS) in the cat. Post-lesion retinal input to the AOS was evaluated using the autoradiographic technique. Unilateral lesion of the lateral terminal nucleus of the AOS (LTN) and the resulting retinal deafferentation of the medial terminal nucleus of the AOS (MTN) induced a spontaneous nystagmus in the dark whose slow phase was directed ipsilaterally to the lesion. VOR gain was reduced for both directions with a maximal decrease for stimulation directed ipsilaterally to the lesion. OKN gain obtained for both directions of binocular stimulation was decreased, mainly when the stimulus was directed contralaterally to the lesion. After two postoperative weeks, spontaneous nystagmus disappeared and the VOR symmetry recovered simultaneously. A symmetrical OKN was only observed after one month. In spite of the known visual selectivity for vertical direction in LTN-MTN cells, the results of this study support a functional involvement of these nuclei in horizontal VOR and OKN.
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  • 31
    ISSN: 1590-3478
    Keywords: Cat ; area 18 ; classification criteria ; receptive field types
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Description / Table of Contents: Sommario È noto che non tutti i campi recettivi dei neuroni corticali visivi rientrano nelle due grandi categorie delle cellule semplici e delle cellule complesse. Pertanto, quei campi recettivi che non presentano proprietà ben definite o solo intermedie a quelle delle cellule semplici e complesse da alcuni autori vengono considerati semplici e da altri complessi. Queste incertezze classificatorie dipendono dal fatto che non esiste un unico schema di classificazione dei neuroni corticali visivi, poiché i due schemi attualmente più seguiti, quello di Hubel e Wiesel e quello di Bishop, vengono considerati non comparabili essendo il primo uno schema qualitativo basato sull'uso di stimoli luminosi stazionari ed il seconda uno schema quantitativo basato sull'uso di stimoli luminosi in movimento. Campi recettivi che non posseggono le proprietà tipiche delle cellule semplici e complesse sono stati osservati nel gatto oltre che nell'area 17 anche nell'area 18. I vari campi recettivi registrati in quest'ultima area sono stati analizzati sia qualitativamente che quantitativamente usando i criteri di classificazione dei due schemi attualmente esistenti. È stato osservato che, almeno per quanto riguarda le cellule semplici, tali schemi di classificazione dei neuroni corticali visivi non sono antitetici ma equivalenti.
    Notes: Abstract There is in vision research a general unwillingness to classify or define visual cortical cell types, particularly new cell types, outside the classical simple/ complex dichotomy. Cells lacking clear-cut characteristics are, therefore, considered simple by some authors and complex by others. The present unsatisfactory state has largely arisen because of the absence of any rigorous, generally accepted, classification scheme of visual cortical neurons. Actually the present two classification schemes of visual cortical neurons, that is the Hubel and Wiesel and the Bishop schemes, are generally considered to be not comparable since the former is based on the cell qualitative static-field properties as revealed by hand-held stationary flashing stimuli, whereas the latter is based on the cell quantitative dynamic-field plotting properties as revealed by moving light stimuli. Since receptive fields lacking clear-cut characteristics of simple and complex cells have been observed in area 18 of the cat as well, all the receptive field types of this area have been classified either qualitatively or quantitatively using both the Hubel and Wiesel and the Bishop classifying procedures. It has been observed, at least as far as simple cells are concerned, that the two schemes are not antithetic but, on the contrary, equivalent if averaging procedures are taken into consideration.
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  • 32
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 49-58 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Fundamentals of Material Selection in the Conditions of Erosive WearProblems of proper selection of materials for parts subjected to wear by a stream of abrasive particles are discussed. Considering the main laws governing such kind of wear, the author concludes that target material selection in the case of erosion, like in any other case of abrasive wear, will depend on the ratio of abrasive grain hardness to material hardness. Special attention should be given to hard components in the abrasive. It has been established that a 10-15% content of quartz particles in the abrasive is enough to cause an abrupt fall in the wear resistance of chilled steels, white iron and hard surfacing alloys, thus making their use questionable. Finegrained WC-Co-type sintered carbides have shown the highest wear resistance in such conditions.The conclusions drawn in this paper are borne cut by a considerable body of experimental data.
    Notes: In dem Artikel werden Probleme der zweckmäßigen Werkstoffauswahl bei der Strahlverschleißbekämpfung behandelt, die allgemeinen Gesetzmäßigkeiten deser Verschleißart dargelegt und gezeigt, daß analog zu anderen Abrasivverschleißarten auch in diesem Fall die Materialauswahl durch einen Vergleich von Werkstoff- und Schleifkornhärte erleichtert wird. Besondere Aufmerksamkeit gilt dem Einfluß von Zusätzen harter Körner in Strahlmittel. Schon ein etwa 10-15prozentiger Anteil von Quarzteilchen ruft eine jähe Senkung des relativen Verschleißwiderstandes bei gehärteten Stählen, Hartguß und Auftragsschweißwiderstandes bei gehärteten Stählen, Hartguß und Auftragsschweißungen hervor und macht deren Anwendung problematisch. Den größten Verschleißwiderstand unter solchen Bedingungen haben feinkörniger WC-Co-Sinterhartmetalle.Die Schlußfolgerungen werden durch umfangreiche Versuchsergebnisse belegt.
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  • 33
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 95-96 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: A Study on Alloy Element Loss in MIG Welding of Stainless SteelsAAS-analysis of welding fume yields information about alloy element loss in MIG welding of stainless steels. Welding under shielding gases short of oxygen, the heavy metal loss can be correlated with the element's partial pressures in the welding wire alloy.
    Notes: Durch Analyse des Schweißrauches läßt sich Aufschluß über das Abbrandverhalten von Drahtelektroden gewinnen. Beim MAG-Schweißen unter sauerstoffarmen Schutzgasen wird der Schwermetall-Abbrand durch die Partialdrucke der Legierungskomponenten kontrolliert.
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  • 34
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 102-107 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Additional Material: 11 Ill.
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  • 35
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 36
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 109-117 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Influence of Specimen Size on the Fracture Mechanical Behaviour of Sintered SteelFracture mechanics testing was carried out with small and big specimens using high-temperature sintered Fe-2%Cu-2.5%Ni-alloys in the densities of ρ = 7.1 and 7.4 g/cm3. These steels are often used in the manufacturing of PM-parts. Due to the different dismensions the crack propagation is for the bigger sizes faster than for the smaller sizes. Also the conditional fracture toughness of the big specimens is superiour to the toughness of the small specimens. But under consideration of a plain strain state for the big specimens and of a plain stress state for the small specimens valid fracture toughness values being independent from the specimen size can be calculated applying linear-elastic fracture mechanics.These results were obtained for both densities investigated. The increase of the density delivers principally better fracture mechanical data. Hereby the relation of strength data with the microstructure is also discussed.
    Notes: Am Beispiel von in der Formteilherstellung häufig verwendeten hochtemperaturgesinterten Fe-2%Cu-2,5%Ni-Legierungen in den Dichten ρ = 7,1 und 7,4 g/cm3 wurden bruchmechanische Untersuchungen an Klein- und Großproben vorgenommen. Aufgrund der unterschiedlichen Abmessungen ergibt sich bei Großproben eine größere Rißfortschrittsgeschwindigkeit und eine größere vorläufige Bruchzähigkeit als bei den Kleinproben. Durch Zuordnung des ebenen Dehnungszustandes zu den Großproben und des ebenen Spannungszustandes zu den Kleinproben läßt sich jedoch unter Berücksichtigung der jeweiligen plastischen Zonen ein von der Probenform unabhängiger gültiger Bruchzähigkeitswert auf der Basis der linear-elastischen Bruchmechanik berechnen.Diese Ergebnisse gelten für beide Dichtevarianten, wobei die Erhöhung der Dichte die bruchmechanischen Kennwerte grundsätzlich verbessert. Hierbei wird auch auf den Zusammenhang zwischen den Festigkeitskennwerten und dem Gefüge eingegangen.
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  • 37
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. A35 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 38
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 140-148 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Remote Testing of Polymers with Photothermal Analysis of Thermal WavesAfter an introduction to thermal waves a comparison is made of photoacoustic detection methods (gas cell, piezoceramic) and photothermal detection arrangements (front surface and rear surface methods). Previously only photoacoustic methods have been applied to polymer related problems, while the advantages of photothermal measurements - remote and nondestructive evaluation - have been demonstrated on metals. The experimental part of this paper presents first steps to apply photothermal analysis of thermal waves to some problems of polymers: thickness measurement of thin layers; on-surface and subsurface defects; delamination of bonding and coating curing reactions; glass fibre content; orientation of fibres and molecules; aging processes.The present results indicate that the method can be used for nondestructive remote quality assurance of thin layers and foils. Further development is required to apply the method to nondestructive testing of thick walled components.
    Notes: Nach einer Einführung in die Grundlagen von Wärmewellen werden die photoakustischen Meßmethoden (Gaszelle, Piezokeramik) den photothermischen Meßmöglichkeiten (Frontseiten- und Rückseitenmethode) erläuternd gegenübergestellt. Kunststoffbezogene Problemstellungen wurden bisher nahezu ausschließlich mit photoakustischen Methoden bearbeitet. Die Vorteile der photothermischen Messungen - berührungslose und zerstörungsfreie Prüfung - konnten bisher an Metallen verdeutlicht werden. Der experimentelle Teil dieser Arbeit zeigt in ersten Schritten auf, daß auch bei Kunststoffen folgende Problemstellungen mit der Methode der photothermischen Wärmewellenanalyse bearbeitet werden können.Dickenmessung dünner Schichten; äußere und innere Fehlstellen; Haftungsfehler bei Verklebungen oder Beschichtungen; Vernetzungsreaktionen; Glasfaseranteil; Glasfaser- und Molekülorientierungen; Alterungsvorgänge.Die bisherigen Ergebnisse lassen sich in die zerstörungsfreie Qualitätssicherung dünner Schichten und Folien übertragen. Die zerstörungsfreie Prüfung von dickwandigen Bauteilen bedarf einer methodischen Weiterentwicklung.
    Additional Material: 15 Ill.
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  • 39
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. A101 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 40
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 411-415 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Steel of the type 13%Cr6%Ni modified with 0.56%Mo allows to achieve favourable mechanical metallurgy properties, including decrease of the susceptibility to temper embrittlement. Application of two-stage tempering (first at 625°C, second at 575-600 °C) leads to counterbalanced mechanical properties and to the improvement of corrosion resistance in dependence on the modification of structure.The physical metallurgy characteristics were completed by potentiodynamic measurements. It was found that this evaluation indicates very sensitively the formation of austenite in the structure after applying tempering at intercritical temperatures. A model of austenite stabilization using the single and two-stage tempering method is presented.
    Additional Material: 12 Ill.
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  • 41
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 436-436 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 42
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    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 15 (1984), S. A2 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 43
    Electronic Resource
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    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 15 (1984) 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 44
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Finsh and Solid Rolling of Automotive Running Gear and Drive ComponentsAutomotive parts, in particular running gear and drive components, are subject to high dynamic loads in regards to strength.When designing new parts, this is taken into account through dimensioning, material selection and constructional conception. Normally the mentioned measures will not be applied to old designs if, for example, they are subjected later to higher loads because of an increase in engine power output. Only the selection of different materials as well as strength increasing measures and methods remain for these parts.An important method is solid rolling. The examples of completed designs demonstrate the possible strength improvements, influence of rolling force on component strength as well as desired and undesired accompaniments.A comparison is made between solid rolling and other strength improving measures, such as inductive hardening.The results show the solid rolling method to be cost-favorable, very effective and safe in handling. The method has its limits in geometry (open rotation-symmetrical cross sections are required), size (component too large, cross section too filigreed) and application range (temperature) of components.
    Notes: Kraftfahrzeug-Bauteile, insbesondere Fahrwerkskomponenten und Antriebsbauelemente sind festigkeitsmäßig dynamisch hoch beansprucht.Bei der Neukonstruktion wird dem durch Dimension, Werkstoffauswahl und Konstruktionsprinzip Rechnung getragen. An bestehenden Konstruktionen, wenn diese beispielsweise durch spätere Leistungssteigerung höher belastet werden, scheiden in der Regel die genannten Maßnahmen aus. Hier bleiben dann neben anderer Werkstoffwahl nur festigkeitssteigernde Maßnahmen und Verfahren.Als ein bedeutendes Verfahren steht hier das Festwalzen. Die Beispiele ausgeführter Konstruktionen zeigen die möglichen Festigkeitssteigerungen, den Einfluß der Walzkräfte auf die Bauteilfestigkeit sowie erwünschte und unerwünschte Begleiterscheinungen.Es wird verglichen zwischen Festwalzen und anderen Maßnahmen zur Festigkeitssteigerung wie Induktivhärten.Das Ergebnis zeigt das Festwalzverfahren als kostengünstig, sehr wirksam und sicher in der Handhabung. Grenzen liegen verfahrensbedingt in der Geometrie (offene rotationssymmetrische Querschnitte notwendig), Dimension (Bauteil zu groß, Querschnitt zu filigran) und im Einsatzbereich (Temperatur) der Bauteile.
    Additional Material: 10 Ill.
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  • 45
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    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 65-72 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Activation Enthalpies and Mechanisms of Subcritical Crack Propagation in Aluminium Oxide CeramicsProgressive crack propagation has been investigated in the temperature range between 25 and 1000°C for two commercial varieties of Al2O3 ceramic, using double torsion specimens. 3 different temperature regions have been found, each of them with a different dependence of the effective activation enthalpie on the stress intensity factor. While at low temperatures the crack propagation rate is mainly controlled by the reaction of the grain boundary phase with the water vapor partial pressure of the environment, the softening of this phase is the predominent factor at high temperatures.
    Notes: An zwei Qualitäten kommerzieller Al2O3-Keramik unterschiedlichen SiO2-Gehalts wurde an Doppeltorsionsproben die langsame Rißausbreitung im Temperatubereich von 25 bis 1000°C untersucht. Es wurden drei Bereiche gefunden, die eine unterschiedliche Abhängigkeit der effektiven Aktivierungsenthalpien vom Spannungsintensitätsfaktor aufweisen. Bei niedrigen Temperaturen steuert im wesentlichen die Reaktion des Wasserdampfes der umgebenden Luft mit der Korngrenzenphase die Rißausbreitung, bei hohen Temperaturen spielt die Erweichung dieser Korngrenzenphase die entscheidende Rolle.
    Additional Material: 8 Ill.
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  • 46
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Ductility of Metallic Diffusion Type Coatings on Nickel-Based Alloys and its DeterminationA test method is being presented by which ductility properties of metallic diffusion coatings, which are used against hot corrosion e.g. on turbine blades, can be measured. The ductility measurements are based upon the acoustic emission during crack initiation within coated specimens under mechanical load. By plotting the acoustic emission and the stress vs. elongation simultaneously, the crack initiation stress vs. elongation simultaneously, the crack initiation stress of the coating and the 0,2%-proof stress of the substrate can be determined by the same experiment. Correlations between these two stress levels led to ductility characteristics and within the scope of these investigations to dependences on temperature, coating thickness, strain rate and thermal history of the coating/substrate system. The investigations were carried out on three different diffusion coatings combined with two nickel-base superalloys. Ductility measurements up to 850°C led to ductile-brittle-transition-temperatures as well as to temperature dependant stress and strain levels, below which the coatings on certain substrate behave in a ductile manner.
    Notes: Diffusionsschutzschichten gegen Heißgaskorrosion sind vielfach bei niedrigen Temperaturen spröde und werden erst bei höheren Temperaturen zäh. Für das Betriebsverhalten beschichteter Turbinenschaufeln z. B. ist die Kenntnis der Übergangstemperatur vom spröden zum zähen Verhalten von Bedeutung, wobei die Eigenschaften der Schutzschicht vom jeweiligen Trägerwerkstoff beeinflußt werden. - Es wird nun ein Prüfverfahren vorgestellt, mit dem an beschichteten Proben unter mechanischer Beanspruchung das Auftreten erster Anrisse in der Schutzschicht durch Schallemissionsmessungen nachgewiesen und gleichzeitig durch die Aufnahme eines Spannung-Dehnung-Schaubildes die relative Lage der Anrißspannung der Schutzschicht und der 0,2 Grenze des Trägerwerkstoffes erfaßt werden. Aus den durchgeführten Versuchen ließen sich Angaben über die Zähigkeit in Abhängigkeit von der Temperatur und anderen Einflußgrößen wie Schichtdicke, Dehngeschwindigkeit und thermischer Vorgeschichte ableiten. Auf diese Weise konnten für drei verschiedene Schutzschichten, dei mit zwei hochwarmfesten Nickellegierungen kombiniert waren, Spröde Zäh-Übergangstemperaturen bestimmt werden. Weiterhin ergaben sich bis zur höchsten Prüftemperatur von 850°C Spannungs- und Dehnungsgrenzen, unterhalb derer die untersuchten Schutzschichten auf den Trägerwerkstoffen rißfrei bleiben.
    Additional Material: 15 Ill.
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  • 47
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 108-108 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 48
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    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 15 (1984) 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 49
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    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 117-123 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Ergebnisse von Untersuchungen mit einem instrumentierten Kerbschlaghammer an einer Molybdänbasislegierung, Nickelbasislegierungen und Incoloy 800Mit einem instrumentierten Pendelschlagwerk wurden Experimente an der Molybdänbasislegierung TZM, den Nickelbasislegierungen Nimocast 713 LC, Inconel 625, Nimonic 86, Hastelloy S und der Eisenbasislegierung Incoloy 800 durchgeführt. Die Ergebnisse werden unter den Gesichtspunkten der verbrauchten Schlagenergien und der dynamischen Bruchzähigkeit diskutiert.In allen Fällen war die Übereinstimmung zwischen den Energien, die am Schleppzeiger des Hammers abgelesen wurden und den Energien, die durch die Integration des Kraft-Weg Diagrammes ermittelt wurden, ausgezeichnet.Ein Verfahren für die Bestimmung der dynamischen Bruchzähigkeit für eine Last vs. Lastpunktverschiebungskurve mit hohen Oszillationen unter Verwendung einer gemittelten Kurve wurde vorgeschlagen. Verwendet man dieses Verfahren, findet man keinen deutlichen Einfluß der Experimente mit Hammer und Stössel (5,0 m/s und 0,1 m/s) auf die dynamische Bruchzähigkeit. Halbiert man die Fallhöhe, d.h. halbiert man die totale Schlagenergie, so werden die dynamischen Bruchzähigkeitswerte für die Legierungstypen erniedrigt.Niedrige absorbierte Schlagenergien sind oft verknüpft mit hohen Bruchzähigkeitswerten. Hier fehlt die Reserve in der Verformung und/oder im stabilen Rißwachstum.
    Notes: Experiments were performed on the molybdenum base alloy TZM, the nickel base alloys Nimocast 713 LC, Inconel 625, Nimonic 86, Hastelloy S, and the iron base alloy Incoloy 800 with an instrumented impact machine. The results are discussed in terms of absorbed impact energies and dynamic fracture toughness.In all cases the agreement between the energy determined by the dial reading and the energy determined by the integration of the load vs. load point displacement diagram was excellent.A procedure for the determination of the dynamic fracture toughness for load vs. load point displacement diagrams exhibiting high oscillations using an averaged curve is proposed. Using this procedure a pronounced influence of the experiments with tup and chisel (5.0 m/s and 0.1 m/s respectively) on the dynamic fracture toughness is not detectable. Using half the drop height, i.e. halving the total energy, lowers the dynamic fracture toughness values for these types of alloys. Low absorbed impact energies are often combined with high fracture toughness values. In these cases there is no or only a small reserve in deformation and/or stable crack growth.
    Additional Material: 18 Ill.
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  • 50
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 149-153 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Welding in Tank and Plant ConstructionSince a relatively limited number of plastics types are used, the welding tasks involved in chemical apparatus engineering can be accomplished with just a few welding techniques are well-known and welding can be carried out efficiently, reliably and economically by this means. In this respect, however, a number of important principles have to be observed. The DVS guidelines provide vital information on questions relating to calculation, design, personnel, equipment, material and testing. Extrusion welding enjoys prime importance as regards quality and economic aspects.
    Notes: Die Schweißaufgaben im chemischen Apparatebau werden an einer relative geringen Anzahl von Kunststofftypen mit wenigen Schweißverfahren bewältigt. Diese Verfahren sind in ihren Grenzen erfaßt und erlauben sichere und wirtschaftliche Schweißungen. Es sind hierbei allerdings eine Reihe wichtiger Grundsätze zu beachten. Die entsprechenden DVS-Richtlinien geben zu Berechnungs-, Gestaltungs, Personal-, Geräte-, Material- und Prüffragen wesentliche Hinweise. Vorrangige Bedeutung im Hinblick auf Qualität und Wirtschaftlichkeit im Behälter- und Apparatebau hat das Extrusionsschweißen.
    Additional Material: 9 Ill.
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  • 51
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 153-157 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Long Term Testing of Welded Joints from HDPE under Complex LoadingTest methods to determine the long term weld-factors for heated tool butt weldings, extrusion weldings and hot gas weldings are presented. Instead of tensile bars welded pipers are tested under internal pressure to abbreviate the test times. The results of long term creep tests with welded and unwelded PE-HD pipes under the influence of several fluids are also discussed.
    Notes: Für die im Apparate- und Behälterbau am meisten angewandten Schweißverfahren: Heizelementstumpf-, Extrusions- und Warmgas-schweißen werden Prüfmethoden zur Bestimmung der Langzeit-schweißfaktoren vorgestellt. Als Prüfkörper werden hierbei geschweißte Rohre verwendet, um einen mehrdimensionalen Span-nungszustand zu realisieren und die Prüfzeiten zu verkürzen. Desweiteren wird der Einfluß einiger Medien auf geschweißte Rohre im Vergleich mit ungeschweißten Rohren untersucht.
    Additional Material: 6 Ill.
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  • 52
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 183-185 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Experiences in Welding Highly Pure, Gas-Sensitive MaterialsHighly pure steels and non-ferrous react during processing, particularly welding, with atmospheric gases and change their service properties. Hence special measures are often necessary in forming and inert gas welding. Taking the specific example of a high pure chromium steel (superferritic), welding properties, processing data and selection of suitable inert gas torches are described. The possibility of applying this information to other materials such as titanium is discussed.
    Notes: Hochreine Stähle und Nichteisenmetalle reagieren bei der Verarbeitung, insbesondere beim Schweißen mit den Gasen der Luft und verändern ihre Gebrauchseigenschaften. Daher sind vielfach Sondermaßnahmen beim Formieren und Schutzgasschweißen notwendig. Speziell am Beispiel eines Chromstahles hoher Reinheit (Superferrit) werden die Schweißeigenschaften, Daten der Verarbeitung sowie die Auswahl geeigneter Schutzgasbrenner beschrieben. Vergleichende Hinweise und Anwendungsbeispiele für andere Werkstoffe wie z. B. Titan sind möglich.
    Additional Material: 2 Ill.
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  • 53
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 190-190 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 54
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 199-206 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Untersuchungen zum Einfluß der Hammergeschwindigkeit und der Auslagerung auf die dynamische Bruchzähigkeit für Inconel 625Mit einem instrumentierten Pendelschlagwerk wurden Experimente an der Nickelbasislegierung Inconel 625 im Anlieferungszustand und nach Auslagerung über 3,6 Ms (1000 h) bei 923 K (650°C) unter Anwendung unterschiedlicher Fallhöhen durchgeführt. Die verbrauchte Schlagenergie kann sowohl über den Schleppzeiger, über die Integration des Kraft-Lastpunktverschiebungs-Diagrammes als auch aus der Integration des Kraft-Zeit-Diagrammes bei gleichzeitiger Kenntnis der Schlaggeschwindigkeit v0 unmittelbar vor Auftreffen des Hammers auf die Probe ermittelt werden. In allen Fällen ist die Übereinstimmung gut.Es wird gezeigt. -daß die dynamische Bruchzähigkeit abhängig ist von der Hammergeschwindigkeit v0 und damit von der totalen Energie des Hammers bei unterschiedlichen Fallhöhen.-daß die Versprödung infolge Wärmebehandlung nicht mit einer Absenkung der Bruchzähigkeit verbunden ist, obwohl eine starke Abnahme der verbrauchten Schlagenergie beobachtet wird. Definiert man eine dynamische Spannung σ aus der Geschwindigkeitsabhängigkeit der Bruchzähigkeit, so ist σ größer für das versprödete Material im Vergleich zum Anlieferungszustand. Diese Tendenz ist von Zugversuchen her bekannt.-daß die dynamische Bruchzähigkeit mit der absorbierten Schlagenergie bis zum Lastmaximum für das wärmebehandelte Material korreliert werden kann, während für den Anlieferungszustand keine Abhängigkeit gefunden wird.Die Änderung der Hammergeschwindigkeit im Verlauf des Stoßprozesses ist nur klein für diesen Werkstofftyp.
    Notes: Experiments were performed with an instrumented impact machine using different drop heights, on the nickel base alloy Inconel 625 in the as-received state and after heat treatment for about 3.6 Ms (1000 h) at 923 K (650°C).The absorbed impact energy can be obtained either by the direct dial reading, by the integration of the load versus load point displacement diagram or by the integration of the load versus time diagram, knowing the initial impact velocity v0 of the tup. In all cases the agreement was excellent.It is shown that. -the dynamic fracture toughness is dependent on the tup velocity v0 and, as a consequence, on the total energy of the hammer at the different drop heights.-defining a dynamic stress σ from the velocity dependence of the fracture toughness, the stress σ is higher for the embrittled material - a tendency verified by tensile tests.-the dynamic fracture toughness can be correlated with the absorbed impact energy up to the load maximum for the heat treated material while the as-received material exhibits no such dependence.The change in the tup velocity during the impact process is only small for this type of material.
    Additional Material: 8 Ill.
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  • 55
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 56
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    Materialwissenschaft und Werkstofftechnik 15 (1984) 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 57
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 246-250 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Schallemissionsprüfung von Wärmetauschern des Reaktors SaphirDie Schallemissionsanalyse ist eine zerstörungsfreie Prüfmethode, die zur Untersuchung und Überwachung von Strukturen und druckführenden Komponenten verwendet wird. Das Ziel der Messung am 5 MW Forschungsreaktor Saphir war die Untersuchung und Auswertung der hohen Betriebsgeräusche in den Wärmetauschern des Kühl-systems.Die Ergebnisse zeigten, daß von den 9 Wärmetauschern, die in 3 Gruppen angeordnet sind, 5 Wärmetauscher ein hohes Betriebsgeräusch aufweisen. Die Ursache ist auf die Schwingung der Rohrbündel in Wärmetauschern beim Durchfluß des Pool-Wassers zurückzuführen. Die axiale Ortung bestätigte, daß die Geräusche von mehreren Quellen verursacht werden.
    Notes: The acoustic emission technique is a non-destructive testing method used for inspection and surveillance of structures and pressurized components. In particular, the purpose of the measurement on the 5 MW research reactor SAPHIR was to investigate and evaluate the abnormally high noise levels during operation of the heat exchangers of the cooling system.The results showed that 5 heat exchangers out of the total of 9 (assembled in 3 groups) were responsible for the higher noise level. This is probably due to some abnormal vibration of the tube bundles therein, caused by the through-flow of the pool water. Indeed, attempts of localizing the source showed that there must be several, distributed sources.
    Additional Material: 5 Ill.
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  • 58
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 250-256 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Ultrasonic Testing of Metal DepositsThe adhesive strength of Ni-deposits has been determined with the well known ring shear test and by a test procedure which usually is used to analyze the resistance of a material against cavitation. In this case the specimen is fastened at the top of an ultrasonic vibrator and oscillates in an aqueous fluid. The deposit/substrate interface is strengthened by high accelerative forces and by mechanical attack of imploding bubbles in the fluid. It was shown that this method is able to distinguish the effect of different pretreatment of the substrate surface. The test result is given as the duration of attack without any exfoliation of the deposit.
    Notes: Die Prüfung der Haftfestigkeit metallischer Überzüge auf z. B. metallischen Grundwerkstoffen spielt eine wichtige Rolle im Hinblick auf die Funktionalität der beschichteten Bauteile im Betrieb. Ihre Bestimmung ist nicht in einfacher Weise möglich, wenn es gilt, Zahlenwerte zu erhalten. Nachfolgend werden zwei Verfahren vorgestellt, von denen das eine, nämlich der ring-shear-test, schon seit längerer Zeit bekannt ist, das andere jedoch, die Untersuchung mit dem Ultraschallkoppelschwinger, neu entwickelt wurde. Die Heranziehung des ring-shear-testes dient in der vorliegenden Arbeit dem Vergleich, wobei hier bekanntlich Zahlenwerte mit der Dimension einer Spannung erhalten werden, während der Versuch mit dem Ultraschallkoppelschwinger Beständigkeitszeiten als Entscheidungskriterium liefert.Gleichzeitig ließ sich mit beiden Methoden der Einfluß der Vorbehandlung auf die Haftfestigkeit eindeutig nachweisen.
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  • 59
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 257-264 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Statistical Size Effect at Random LoadingResults of random tests are used to show the applicability of the theory of statistical size effect. The specimens of all the tests of this report were made from the aluminium alloy 7075 T 7351. The specimens were machined from plates (2000 × 1000 × 40 mm). The main dimension of the specimens corresponds with the rolling direction. A standard random load sequence of Gaussian type which is recommended for general application in fatigue testing was used as loading program [19].In a first test series notched round bar specimens (Fig. 2) were used to investigate the sequence effect. 30 specimens were tested with the standard load sequence, 30 specimens with the variable load sequence. All the other test conditions were kept constant. Fig. 4 shows that the scatter of lifetime (cycles to fracture) is not influenced by the load sequence.In a second test series flat specimens with central holes were tested (Fig. 5) in order to show the existence of a pure statistical size effect at random loading. If the specimen has 1, 3 or 7 holes and all the other test conditions are kept constant, only the size of the area where cracks can initiate is enlarged. The results which are plotted in Fig. 6 show a very clear size effect. The results of the 1-hole specimen (A = A0) were used to determine the constants of Eq. (5). By inserting A = 3 A0 resp. A = 7 A0 the other test results can be predicted. In a third test series round bar specimens with a circumferential notch with different notch root radius (ρ = 1 mm resp. ρ = 6 mm) were tested (Fig. 2, Table 1). The specimens were loaded in such a way that the maximum stress in the notch root and its time-dependence was equal. In this very common case, the stress integral must be determined by applying Eq. (3). Additional tests to determine k and numerical calculations were necessary to evaluate Eq. (3). The final results are plotted in Fig. 8. By inserting A = A0 resp. A = 5 A0 into Eq. (7) the results can be described.The basis of the applicability of the theory of statistical size effect is the weakest link concept. The examination of the fracture surface and X-ray analyses showed that there was a higher content of iron (Fig. 11) in those regions where the fatigue cracks initiated. It is supposed that inclusions of intermetallic Al-Fe particles are those weakest links in the structure, where fatigue cracks nucleate.
    Notes: Es wurde der Einfluß der Bauteilgröße auf das Anrißlebensdauerverhalten bei zufallsartiger Schwingbeanspruchung an gekerbten Prüfkörpern aus der Al-Legierung AlZnMgCu 1,5 (7075T7351) untersucht. Durch geeignete Prüfkörperwahl gelang eine Trennung des statistischen (Fehlstellenmodell) und des spannungsmechanischen (Stützwirkungsmodell) Effekts und damit der Nachweis des rein statistischen Einflusses der Baugröße. Darüber hinaus wurde gezeigt, daß das auf dem Fehlstellenmodell beruhende Rechenverfahren auch bei Änderung der Stützwirkung im Bauteil seine Gültigkeit bewahrt. Der Begriff der Fehlstelle konnte durch eine konkrete mikrostrukturelle Werkstoffinhomogenität ersetzt werden. Diese zufällig im Material verteilten Fehler werden als Ursache für die Lebensdauerstreuung angesehen. In diesem Zusammenhang konnte für eine auf einem stationären Gaußprozeß beruhende Lastfolge geklärt werden, daß die Lebensdauerstreuung nicht von der Lastspielreihenfolge abhängt, wenn das Beanspruchungskollektiv und der zeitliche Charakter des Lastablaufs erhalten bleiben.
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. A65 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 309-314 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Oszillationen des Korrosionspotentials bei rostfreien StählenDie Korrosionspotentiale von rostfreien Stählen in chloridhaltigen Lösungen sind in Umgebungen, in denen weder Lochfraß noch Spaltkorrosion auftreten, konstant. In diesen Fall sind die Korrosionspotentiale weitgehend unabhängig von der Temperatur und der Chloridionkonzentration. Bei Stählen mit abnehmendem Korrosions widerstand oder mit zunehmender Temperatur und zunehmender Chloridionkonzentration tritt eine Situation ein, bei der das Korrosionspotential zu oszillieren beginnt - und zwar zwischen zwei Werten, die ungefähr dem Lochfraßpotential Ep und dem Repassivierungspotential Epp entsprechen. Diese Potentialoszillationen sind häufig von Lochfraß und Spaltkorrosion begleitet; andererseits gibt es Fälle, bei denen sogar nach langer Zeit kein Korrosionsanriß sichtbar ist. Die Oszillationen werden einem instabilen Passivitätsverhalten zugeschrieben.
    Notes: The corrosion potentials of stainless steels in chloride solutions for conditions significantly removed from those leading to pitting and crevice corrosion are constant and to a first approximation largely independent of temperature and chloride ion concentration. With increasing temperature and/or chloride ion concentration or with decreasing corrosion resistance there comes a situation when the corrosion potential begins to oscillate, between two and values roughly corresponding to Ep and Epp. These potential oscillations are often associated with pitting and crevice corrosion, although there are clear cases when no corrosion attack was visible even after prolonged exposure. The oscillations are attributed to unstable passivity.
    Additional Material: 9 Ill.
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 323-330 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: On the Interaction between Work-Material and Forming-Process and its Investigation by ExperimentsExperiments are described and discussed for determining material properties before metal forming as well as process parameters during the metal forming operation and workpiece properties after metal forming.Before metal forming “pure” properties of matter have to be determined which in many cases is achieved by standardized testing methods. During and after the forming operation, however, the testing methods of interest are not yet standardized to the same extent. In particular it is necessary after metal forming, to take into account the effect of geometry on the workpiece properties which results into modified conditions for testing material and workpiece properties.
    Notes: Es werden Versuche beschrieben und diskutiert, in denen Werkstoffeigenschaften vor dem Umformvorgang, Verfahrensparameter während der Umformung sowie Werkstoff- und Werkstückeigenschaften nach der Umformung erfaßt werden können.Zur Bestimmung von Werkstoffeigenschaften vor der Umformung stehen zahlreiche genormte oder sonstwie vereinheitlichte Prüfverfahren zur Verfügung. Dies ist bei Versuchen während und nach der Umformung nicht in gleichem Maße der Fall. Insbesondere muß nach der Umformung der Einfluß der Geometrie auf die Werkstückeigenschaften berücksichtigt werden, wodurch sich veränderte Bedingun-gen für Versuche zur Erfassung von Werkstoff- und Werkstückeigenschaften ergeben.
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 359-362 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Additional Material: 2 Ill.
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. A83 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 65
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 371-377 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Bruchenergiemessungen an keramischen WärmedämmschichtenDie Bruchenergie von plasmagespritzten Wärmedämmschichten aus ZrO2 · MgO, ZrO2 · Y2O3, ZrO3 · CaO · Al2O3 und Al2O3 · TiO2 auf Metallsubstraten wurde sowohl für einen Adhäsionsbruch als auch für einen Kohäsionsbruch der Deckschichten mit Hilfe gekerbter Schichtverbundbiegeproben ermittelt. Die verallgemeinerte Energiefreisetzungsrate wurde als Maß für die Bruchenergie benutzt. Sie berücksichtigt die in der Kraft-Durchbiegungskurve der Proben auftretende Nichtlinearität. Das Versagen der Proben innerhalb der Deckschicht oder in der Grenzfläche wird von der Bildung und Vereinigung von sekundären Rissen in der Deckschicht begleitet. Diese Vorgänge verursachen das nichtlineare Verformungsverhalten und eine von der Rißgeschwindigkeit abhängige Bruchmorphologie.
    Notes: The fracture energy of plasma-sprayed thermal barrier coatings of ZrO2 · MgO, ZrO2 · Y2O3, ZrO2 · CaO · Al2O3, and Al2O3 · TiO2 on metal substrates is obtained for both adhesive and cohesive failure modes of the coatings using notched layer-bonded bend test specimens. The generalized energy release rate was employed as a measure of the fracture energy. It takes account of the nonlinearity found in the load-deflection curves of the specimens. The failure of the specimens within the coating or at the interface is accompanied by the formation and linking of secondary cracks in the coating. This causes the non-linearity in the deformation behaviour and a rate-dependent failure morphology.
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 402-402 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. A93 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 416-420 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Improvement of Fatigue Properties by Roll PeeningWith sophisticated calculations a better understanding of the roll peening process is possible. Calculations together with experimental determination of the fatigue properties allow for a reduced test program to determine the fatigue limit of specimens with similar geometrical shape.
    Notes: Mit Hilfe verbesserter Berechungsverfahren lassen sich vertiefte Erkenntnisse über die Vorgänge beim Festwalzen gewinnen. Darüber hinaus bietet die rechnerische Analyse der Vorgänge zusammen mit der experimentellen Ermittlung der Schwingfestigkeit die Möglichkeit einer Übertragbarkeit auf andere Werkstoffzustände und Proben - bzw. Kerbformen. Hierdurch lassen sich Einsparungen durch verminderten Versuchsaufwand erreichen.
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    Materialwissenschaft und Werkstofftechnik 15 (1984), S. 436-436 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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    Particle and Particle Systems Characterization 1 (1984), S. 7-13 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: In the application and the development of on-line methods for particle size analysis one has to distinguish three principally different problem areas:aallocation and preparation of a representative sample,banalysis of the sample,cevaluation of the results.Methods and problems connected with these areas will be discussed in this paper. Some of the methods available for rapid response analysis of particle size distributions mark the beginning of a new era of particle size analysis. One has to recognize however that a uniform solution of the problems of on-line particle size analysis is extremely difficult if not impossible to find. The boundary conditions vary to such an extent that similar methods or combinations of methods can rarely be used in different cases. Since instrument manufacturers will in most cases not be able to adopt their instruments to different industrial applications, specialists will have to solve the problem. One has to recognize, however, that not all of the steps described in this paper have been investigated to an extent which renders possible appropriate solutions. There is still room for improvement.
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    Particle and Particle Systems Characterization 1 (1984), S. 22-27 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: For some time studies have been made relating the values obtained from simple shape description to bulk powder properties. More recently the detailed mathematical description of particle outline has become possible and quite powerful techniques have been developed. These techniques may be used for the regeneration by computer of the shape and, more importantly, for studies relating shape to individual particle behaviour and to bulk powder properties. Quite inadequate attention has been directed to the task of obtaining from the laboratory sample of the bulk powder a representative sample of shapes without bias. In this communication the considerations to be included in the sampling procedure are reviewed and a possible solution to the problems posed is presented.
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    Particle and Particle Systems Characterization 1 (1984), S. 28-31 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: The currently used methods of sample preparation are examined and found to be unsatisfactory in case of counting methods for particle size analysis. It is the purpose of this paper to review the results of investigations of two different measuring principles (light extinction and electrical resistance change) by use of the same signal handling equipment. The commonly used techniques and units are compared with regard to the resulting density distributions of particle size below 0.25 mm. The final conclusions including recommendations to the use of ultrasonic treatment and to improvements of the sampling and the sample-feeding units are valid for all counting methods.
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    Particle and Particle Systems Characterization 1 (1984), S. 53-58 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: When performing particle size analysis by scattered light, coincidences in the measuring volume of optical particle counters not only cause too small a particle concentration to be measured, but also a size distribution to be obtained which is systematically shifted towards coarser particle sizes. It is pointed out in this paper how this shift can be precalculated when the true distribution is given. The results show under which conditions a correction of the measured distribution is indispensable.
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    Particle and Particle Systems Characterization 1 (1984), S. 78-84 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: The classification of powders into groups possessing specific behavioural identities has long been recognized as desirable. This has been approached by describing different powders using two variables and plotting the data on a scatter diagram. The property of interest is then inferred from a powder's position on the scatter diagram. Unfortunately, a powder's behaviour is rarely adequately described by only two variables. To describe a powder more fully requires more variables and this presents a problem in interpretation. Cluster analysis refers to a range of techniques for interpreting multivariate data sets and is used in many fields. This paper describes cluster analysis and considers the method and potential of its application to particle technology. By way of an illustration, a cluster analysis has been performed on twenty-seven powders resulting in groups recognizable by their characteristic fluidisation and flow properties. It is concluded that cluster analysis could be a powerful tool in predictive and analytical work in the field of particle technology.
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    Particle and Particle Systems Characterization 1 (1984), S. 127-131 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Combined gravitational and centrifugal sedimentation analysis was studied using a Sedigraph X-ray sedimentometer and a Ladal pipette centrifuge. The test powders were talc, calcite and lead oxide. The purpose of the study was to examine the possibilities of extending the sedimentation analysis towards finer sizes by the use of centrifugal force. All the test samples could be analysed down to 0.04-0.05 μm by the combined sedimentation procedure with reasonable accuracy and the results were matched to give a uniform distribution. It was also shown to be preferable to present the size analysis data in a log-probability scale, as it gives the means to easily distinguish materials with different particle size characteristics and to estimate the actual distribution by a statistical function.
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    Particle and Particle Systems Characterization 1 (1984), S. 121-126 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: It is often necessary to carry out sedimentation analysis of powders, consisting of two or more components, which differ in some physical properties. By means of theoretical studies of twocomponent systems the systematic errors of the measured particle size distributions were analysed for the case that differences exist in the following combinations of properties:-particle size distribution D(x) and solid density ϱs-D(x) and mass absorption coefficient μm-D(x) and ϱs and μmUsing real systems (SiO2 + Fe2O3, Al2O3 + SiO2, Al2O3 + Fe2O3) the partial and total errors were estimated and compared with the results obtained with a Sedigraph. Differences in the density of the components often result in negligible errors, even for the system SiO2 + Fe2O3, if the mass portion of one component is below about 10%. For the total error the differences of μm and D(x) are decisive. Its value is below 1% if the mass portion of the slightly absorbing component is 〈5% or if the strongly absorbing component is 〈1%.
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    Particle and Particle Systems Characterization 1 (1984), S. 143-152 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: This paper deals with the influence of particle shape and particle size distribution on the fluidisation behaviour of granular activated carbon in the aqueous phase. Methods for relating the degree of expansion, as a function of liquid velocity, to particle shape and particle size distribution are discussed and tested. Two different types of activated carbon, both containing irregularly shaped particles but with differences in shape, are used to test the models discussed. A tentative method which takes into account the influence of water temperature on fluidisation behaviour is proposed.
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    Particle and Particle Systems Characterization 1 (1984), S. 171-177 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Experimental methods to determine minimum sintering temperatures of a variety of granules such as polymers, glass, coal, inorganic salts, etc. are presented. These methods include the use of a dilatometer in which the contraction-dilation characteristics of a small sample is measured, a differential scanning calorimeter test and an Instron machine by which yield strengths are measured. It is clearly shown that for the majority of materials studied, the different methods give similar values for the minimum sintering temperature but that the dilatometer experiment is the simplest as well as the most reliable method. Since the minimum sintering temperature is always less than the solid's melting point, an efficient method of measuring this temperature is very important for all fluidizable granules subjected to high temperatures. The danger of agglomeration during fluidization increases tremendously at temperatures higher than minimum sintering and therefore special precautions must be taken to avoid defluidization under these conditions.
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    Journal of High Resolution Chromatography 7 (1984), S. 147-148 
    ISSN: 0935-6304
    Keywords: Liquid chromatography ; HPLC ; Racemate separation ; β-Cyclodextrin stationary phase ; Cyclohexylphenylglycolic acid ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
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    Journal of High Resolution Chromatography 7 (1984), S. 158-159 
    ISSN: 0935-6304
    Keywords: Multi-mode liquid chromatography ; Adsorption chromatography ; Size exclusion chromatography ; Phenyl-bonded phase ; Styrene oligomers ; Polystyrene polymers ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
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    Journal of High Resolution Chromatography 7 (1984) 
    ISSN: 0935-6304
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
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    Journal of High Resolution Chromatography 7 (1984), S. 160-161 
    ISSN: 0935-6304
    Keywords: Liquid chromatography HPLC ; Bonded phases ; 3,5-Dinitrobenzamidopropyl silica gel ; Charge transfer interaction ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
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    Journal of High Resolution Chromatography 7 (1984), S. 327-327 
    ISSN: 0935-6304
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
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    Journal of High Resolution Chromatography 7 (1984), S. 329-332 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Fused silica capillary columns ; Deactivation ; Polymethylhydrosiloxanes ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
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    Journal of High Resolution Chromatography 7 (1984), S. 338-339 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Pesticides ; Multidetection ; ECD-NPSD-SSD ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 3 Ill.
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    Journal of High Resolution Chromatography 7 (1984), S. 301-305 
    ISSN: 0935-6304
    Keywords: Capillary gas chromatography ; Whisker-walled open tubular columns ; PNA-hydrocarbons ; XAD-2 ; Azaarenes ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A modified clean-up of polynuclear aromatic (PNA) hydrocarbons on XAD-2 is described. n-Alkanes (C16—C28) are separated quantitatively from the PNA hydrocarbons and are eluted in one fraction. The distribution of 17 PNA hydrocarbons and four of their alkyl derivatives, two S-heterocyclic compounds and two azaarenes between the different fractions is reported. Azaarenes containing three rings are separated from PNA hydrocarbons and S-heterocyclic compounds. Whisker-walled open tubular columns coated with OV-215 and OV-25 were used in the separation of isomeric azaarenes and in PNA hydrocarbon profile analysis, respectively. The preparation of such columns is described in detail. Rinsing of capillary columns with cold, concentrated HCI after whisker growth removes much larger amounts of boron and sodium than subsequent leaching with HCI at 180°C. Whisker-walled open tubular columns are successfully applied to the characterization of isomeric benzofluoranthenes and other PNA hydrocarbons isolated from air particulate matter.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 87
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 319-326 
    ISSN: 0935-6304
    Keywords: Capillary GC ; Band broadening in space ; Flooded column inlet ; Retention gap ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: In on-column or in splitless injection with recondensation of the solvent, the length of the flooded zone in the column inlet depends primarily on the wettability of the internal wall of the inlet. For columns with a coated inlet this explains why peak distortion due to band broadening in space by a certain sample volume is pronounced in one case and hardly observable in another. Glass or fused silica capillaries silylated with diphenyltetramethyldisilazane were found to give optimal retention gaps. They combine thorough and thermostable deactivation with good wettability and low retention power. On the other hand it is very easy to deactivate fused silica capillaries with Carbowax. The resulting retention gaps are suitable for a wide range of applications and are particularly attractive for the analysis of dirty samples which require frequent replacement of the inlet.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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  • 88
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 332-333 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Capillary columns ; Polarity mixtures ; Reaction products ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
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  • 89
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 336-337 
    ISSN: 0935-6304
    Keywords: Ion chromatography ; Multidimensional column ; Borophosphosilicate glass (BPSG) film ; VLS ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 90
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 342-343 
    ISSN: 0935-6304
    Keywords: Gas-liquid chromatography ; Logarithmic retention index ; Equation for the calculation of column efficiency ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Tab.
    Type of Medium: Electronic Resource
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  • 91
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984) 
    ISSN: 0935-6304
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 92
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 433-435 
    ISSN: 0935-6304
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 93
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 370-374 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Trace analysis ; On-column injection ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Large sample volume on-column injection (up to 250 μL) of n-pentane solutions of halogenated hydrocarbons has been employed for the direct measurement of both low-boiling and high-boiling compounds in what is essentially a single run. Two-bonded phase, fused-silica capillary columns are joined in series, through which the low-boiling compounds are first chromatographed and detected with an electron capture detector. High-boiling compounds are then trapped in a section joining the two columns, and subsequently chromatographed in the second column, using the same detector. This procedure permits analysis at the ppt level.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
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  • 94
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 404-410 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Multidimensional capillary columns ; Enantiomeric separations ; Intermediate trapping ; Mixed polarities ; Terpene alcohols ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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  • 95
    ISSN: 0935-6304
    Keywords: Low and high resolution liquid chromatography ; Gas chromatography ; Capillary columns ; Alkali flame detection ; Chemical ionization mass spectrometry ; Nitro-PAHs ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: An analytical procedure is described for the fractionation of organic compounds present in environmental samples and the determination of nitro polyaromatic hydrocarbons (nitro-PAHs). Both low and high resolution liquid chromatography are employed for the prefractionation of the soluble organic fraction (SOF) extracted from particulate matter or gaseous pollutants collected on adsorption traps. High resolution gas chromatography is used to analyze four fractions containing alkanes, PAHs, nitro-PAHs, and other polar PAHs. Nitrogen-containing species are separated by GC and detected specifically using an alkali flame (NPD) detector. Flame ionization (FID) detection, GC-MS of positive ions, and negative ion chemical ionization MS of the whole fraction is used for the identification and quantitation of the various components. The composition of SOF extracted from particulate matter emitted from diesel exhausts is elucidated and a large number of nitro-PAHs identified by the combination of the various techniques.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
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  • 96
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984) 
    ISSN: 0935-6304
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 97
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 509-514 
    ISSN: 0935-6304
    Keywords: Gas chromatography, GC ; OV-1/FFAP mixed phase, high-temperature ; silylated glass capillary ; Polar phase-coated HTS capillary ; Golay curves of mixed phases ; Thermal and long-term stability of OV-1/FFAP ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: As an alternative to acid pretreated UCON and FFAP capillaries for the analysis of wide-boiling free fatty acid mixtures, OV-1 : FFAP phase mixtures were used on high-temperature silylated inert glass capillary columns. The HETP-carrier gas velocity curves, peak asymmetry factors, coating efficiency, gas phase and stationary phase contributions to the mass transfer resistance were determined for various OV-1 : FFAP ratios. Mixed-phase capillaries showed optimum performance at a 2 : 1 OV-1 : FFAP ratio. The thermal and long-term stability of OV-1-stabilized FFAP columns surpassed those of the UCON and pure FFAP reference column used.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 98
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 531-532 
    ISSN: 0935-6304
    Keywords: Gas chromatography, GC ; Capillary columns ; Retention gaps ; Large sample volumes ; Flooded zone ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
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  • 99
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 529-531 
    ISSN: 0935-6304
    Keywords: Capillary electrophoresis ; High resolution separation ; High speed analysis ; Dansyl amino acids ; Fluorescamine labeled peptides ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 100
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 536-537 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Capillary column ; On-Column injection ; Vaporizing injection ; Decomposition ; α-Ferrocenyl carbinols ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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